Irradiation of Tungsten Light: A Useful Energy Source for Synthesis of 4,5-Dihydro-pyrazole-1-carbaldehyde Derivatives

In the present communication, reported the easy, convenient route for the synthesis of N-formyl pyrazolines from α, β-unsaturated ketone. The aqueous 2-methoxyethanol was used as reaction media for the synthesis of titled compounds. All synthesized compounds were confirmed on the basis of IR,&nb...

Descripción completa

Detalles Bibliográficos
Autor: Zangade, Sainath
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2017
País:Brasil
Institución:Universidade Federal de Mato Grosso do Sul (UFMS)
Repositorio:Orbital - The Electronic Journal of Chemistry (Campo Grande)
Idioma:inglés
OAI Identifier:oai:periodicos.ufms.br:article/16458
Acceso en línea:https://periodicos.ufms.br/index.php/orbital/article/view/16458
Access Level:acceso abierto
Palabra clave:aqueous 2-methoxyethanol
hydrazine hydrate
irradiation of tungsten light
N-formyl-2-pyrazoline
α,β-unsaturated ketone
Descripción
Sumario:In the present communication, reported the easy, convenient route for the synthesis of N-formyl pyrazolines from α, β-unsaturated ketone. The aqueous 2-methoxyethanol was used as reaction media for the synthesis of titled compounds. All synthesized compounds were confirmed on the basis of IR, 1H NMR, 13C NMR and CHN analysis. DOI: http://dx.doi.org/10.17807/orbital.v9i4.1010