Irradiation of Tungsten Light: A Useful Energy Source for Synthesis of 4,5-Dihydro-pyrazole-1-carbaldehyde Derivatives

In the present communication, reported the easy, convenient route for the synthesis of N-formyl pyrazolines from α, β-unsaturated ketone. The aqueous 2-methoxyethanol was used as reaction media for the synthesis of titled compounds. All synthesized compounds were confirmed on the basis of IR,&nb...

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Bibliographic Details
Author: Zangade, Sainath
Format: article
Status:Published version
Publication Date:2017
Country:Brasil
Institution:Universidade Federal de Mato Grosso do Sul (UFMS)
Repository:Orbital - The Electronic Journal of Chemistry (Campo Grande)
Language:English
OAI Identifier:oai:periodicos.ufms.br:article/16458
Online Access:https://periodicos.ufms.br/index.php/orbital/article/view/16458
Access Level:Open access
Keyword:aqueous 2-methoxyethanol
hydrazine hydrate
irradiation of tungsten light
N-formyl-2-pyrazoline
α,β-unsaturated ketone
Description
Summary:In the present communication, reported the easy, convenient route for the synthesis of N-formyl pyrazolines from α, β-unsaturated ketone. The aqueous 2-methoxyethanol was used as reaction media for the synthesis of titled compounds. All synthesized compounds were confirmed on the basis of IR, 1H NMR, 13C NMR and CHN analysis. DOI: http://dx.doi.org/10.17807/orbital.v9i4.1010