Esterification of free fat acids from waste cooking oil using BiVO4 photocatalysts under visible irradiation.

Herein, we report the FFA photoesterifcation of waste cooking oil (WCO) using a BiVO4 and visible irradiation. Despite undergoing treatments under diferent temperatures (120 °C and 150 °C), both synthesized samples presented high crystallinity and similar morphologies, corresponding to a mixture com...

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Detalhes bibliográficos
Autores: CRISOSTOMO, C. A. B., DAMACENO, F. B., MESQUITA, J. P. de, TORRES, J. A., RIBEIRO, C., RIBEIRO, R. A., LOPES, O. F., AVANSI JR, W., ALMEIDA, J. S., MOURÃO, H. A. de J. L.
Formato: artículo
Estado:Versión publicada
Fecha de publicación:2025
País:Brasil
Recursos:Empresa Brasileira de Pesquisa Agropecuária (Embrapa)
Repositorio:Repositório Institucional da EMBRAPA (Repository Open Access to Scientific Information from EMBRAPA - Alice)
Idioma:inglés
OAI Identifier:oai:www.alice.cnptia.embrapa.br:doc/1177312
Acesso em linha:http://www.alice.cnptia.embrapa.br/alice/handle/doc/1177312
https://doi.org/10.1007/s11144-025-02808-0
Access Level:acceso abierto
Palavra-chave:Bismuth vanadate
Waste cooking oil
Free-fat acids
Photoesterifcation
Ethyl esters
Fatty acid ethyl esters
Descrição
Resumo:Herein, we report the FFA photoesterifcation of waste cooking oil (WCO) using a BiVO4 and visible irradiation. Despite undergoing treatments under diferent temperatures (120 °C and 150 °C), both synthesized samples presented high crystallinity and similar morphologies, corresponding to a mixture composed of the scheelite structure of monoclinic and tetragonal phases of BiVO4. The FFA conversions with the photocatalysts were signifcantly higher than the non-catalytic reactions. The gas chromatography analysis shows that the products are composed of a mixture of ethyl esters and a low amount of fatty acid ethyl esters (FAEE). The results demonstrate that the photoesterifcation of FFA of non-edible vegetable oils can be driven by BiVO4 photocatalysts under visible irradiation, at regular temperature, reduced ethanol/oil molar ratio, and