Detection of anorexigen and benzodiazepinic drugs in weigth reducers compounded formulations and analysis on label contents adequacy by Pharmacognosy Laboratory - Instituto Adolfo Lutz, from June 2004 to March 2007

Obesity has turned to be an important public health issue in Brazil. Nowadays, there are many products so called “weight reducer compounded pharmaceuticals” claiming effectiveness as weight reducers. From June 2004 to March 2007, the Pharmacognosy Laboratory of Instituto Adolfo Lutz analyzed 22 samp...

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Detalles Bibliográficos
Autores: Yano, Helena Miyoco, Santos, Ana Paula, Bugno, Adriana, Auricchio, Mariângela Tirico
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2008
País:Brasil
Institución:Instituto Adolfo Lutz
Repositorio:Revista do Instituto Adolfo Lutz (Online)
Idioma:portugués
OAI Identifier:oai:ojs.periodicos.saude.sp.gov.br:article/32795
Acceso en línea:https://periodicos.saude.sp.gov.br/RIAL/article/view/32795
Access Level:acceso abierto
Palabra clave:weight reducer product
anorexigen
benzodiazepinic
detection limit
comparative thin layer chromatography
fraud
produto emagrecedor
anorexígeno
benzodiazepínico
limite de detecção
cromatografia em camada delgada comparativa
fraude
Descripción
Sumario:Obesity has turned to be an important public health issue in Brazil. Nowadays, there are many products so called “weight reducer compounded pharmaceuticals” claiming effectiveness as weight reducers. From June 2004 to March 2007, the Pharmacognosy Laboratory of Instituto Adolfo Lutz analyzed 22 samples of compounded pharmaceuticals formulations in order to identify anorexigenic drugs (diethylpropione, fenproporex, mazindol and benzodiazepinic) drugs: (chlordiazepoxide, clonazepam, diazepam, bromazepam and lorazepam). The analysis was carried out using comparative thin layer chromatography technique. The label contents were also evaluated in accordance with Brazilian legislation. Detection limit was established to each analyzed compound in accordance with the respective reference standards. Although compound combination of anorexigen, benzodiazepinic and laxative agents are forbidden by Brazilian laws, three out 22 samples were positive for diethylpropione or diazepam with fenproporex. In addition, these substances were not mentioned in the label content. Sixteen samples were in disagreement regarding to the labeling requirements for omitting essential information. These findings showed that much concerns have to be taken by the rule authorities on these compounded pharmaceuticals in order to avoid harmful misuse.