Structural and morphological characterization of rare earth modified lead titanate

Rare earth modified lead titanate powders Pb1-xRExTiO3 (REPT), x = 0.01, 0.05, 0.07 and RE = Yb, Y, were prepared by the Pechini method. The materials were calcined under flowing oxygen at different temperatures from 300 to 700 ºC. Nanostructured REPT were investigated using X-ray diffraction, scann...

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Detalles Bibliográficos
Autores: Lemos, F. C. D., Melo, Dulce Maria de Araújo, Lima, P. S. de, Paskocimas, Carlos Alberto, Silva, Elson Longo da, Silva, J. E. C. da
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2007
País:Brasil
Institución:Universidade Federal do Rio Grande do Norte (UFRN)
Repositorio:Repositório Institucional da UFRN
Idioma:inglés
OAI Identifier:oai:repositorio.ufrn.br:123456789/32259
Acceso en línea:https://repositorio.ufrn.br/handle/123456789/32259
Access Level:acceso abierto
Palabra clave:PbTiO3
Terra Rara
Perovsquita
Método Pechini.
Descripción
Sumario:Rare earth modified lead titanate powders Pb1-xRExTiO3 (REPT), x = 0.01, 0.05, 0.07 and RE = Yb, Y, were prepared by the Pechini method. The materials were calcined under flowing oxygen at different temperatures from 300 to 700 ºC. Nanostructured REPT were investigated using X-ray diffraction, scanning electron microscopy and surface area analysis (BET). The results suggest that the modifier cation incorporated into the system has notable influence in the microstructure and a notable decrease in the crystallite sizes