Determination of furan levels in commercial samples of baby food from Brazil and preliminary risk assessment

Commercial baby food samples available on the Brazilian market (n¼31) were analysed for furan content using a gas chromatography-mass spectrometry method preceded by solid-phase microextraction. A limit of detection of 0.7 mgkg 1, a limit of quantitation of 2.4 mgkg 1, mean recoveries varying from 8...

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Detalles Bibliográficos
Autor: Arisseto, A. Pavesi; et al.
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2010
País:Brasil
Institución:Instituto de Tecnologia de Alimentos (ITAL)
Repositorio:Repositório do Instituto de Tecnologia de Alimentos
Idioma:inglés
OAI Identifier:oai:http://repositorio.ital.sp.gov.br:123456789/671
Acceso en línea:http://repositorio.ital.sp.gov.br/jspui/handle/123456789/671
Access Level:acceso abierto
Palabra clave:Gas chromatography-mass spectrometry (GC-MS);
Solid-phase microextraction (SPME)
Descripción
Sumario:Commercial baby food samples available on the Brazilian market (n¼31) were analysed for furan content using a gas chromatography-mass spectrometry method preceded by solid-phase microextraction. A limit of detection of 0.7 mgkg 1, a limit of quantitation of 2.4 mgkg 1, mean recoveries varying from 80% to 107%, and coefficients of variation ranging from 5.6% to 9.4% for repeatability and from 7.4% to 12.4% for within-laboratory reproducibility were obtained during an in-house validation. The levels of furan found in the samples were from not detected to 95.5 mgkg 1. Samples containing vegetables and meat showed higher furan levels as compared with those containing only fruits. An exposure assessment showed furan intakes up to 2.4 mgkg 1 body weight day 1 (99th percentile) for babies fed exclusively with commercial baby foods. Margins of exposure obtained from intakes estimated in this work indicated a potential public health concern.