Carboxylate-Bridged Copper(II)-Lanthanide(III) Complexes [{Cu3Ln2(oda)6(H2O)6}.12H2O]n (Ln = Dy, Ho, Er, Y; oda = oxydiacetate

The hydrothermal reaction of Ln2O3 (Ln = Dy and Ho), Cu(OAc)2·2H2O, and oxydiacetic acid in the approximate mole ratio of 1:3:8 resulted in the formation of two new members of the isostructural series of polymers formulated as [{Cu3Ln2(oda)6(H2O)6}·12H2O]n, crystallizing in the hexagonal crystal sys...

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Detalles Bibliográficos
Autores: Rizzi, Alberto Claudio, Calvo, Rafael, Baggio, Ricardo Fortunato, Garland, María Teresa, Peña, Octavio, Perec, Mireille
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2002
País:Argentina
Institución:Consejo Nacional de Investigaciones Científicas y Técnicas
Repositorio:CONICET Digital (CONICET)
Idioma:inglés
OAI Identifier:oai:ri.conicet.gov.ar:11336/30088
Acceso en línea:http://hdl.handle.net/11336/30088
Access Level:acceso abierto
Palabra clave:Epr
Cu(Ii)
Lanthanides
Complexes
https://purl.org/becyt/ford/1.4
https://purl.org/becyt/ford/1
Descripción
Sumario:The hydrothermal reaction of Ln2O3 (Ln = Dy and Ho), Cu(OAc)2·2H2O, and oxydiacetic acid in the approximate mole ratio of 1:3:8 resulted in the formation of two new members of the isostructural series of polymers formulated as [{Cu3Ln2(oda)6(H2O)6}·12H2O]n, crystallizing in the hexagonal crystal system, space group P6/mcc (No. 192). Temperature-dependent magnetic susceptibilities and EPR spectra are reported for the heterometallic compounds Cu−Dy 1, Cu−Ho 2, Cu−Er 3, and Cu−Y 4. The results are discussed in terms of the structure of the compounds, the electronic properties of the lanthanide ions, and the exchange interactions between the magnetic ions.