Comparative study of three methodologies saponins quantitative extraction of melisa officinalis “toronjil”

In our research, a phytochemical screening was performed by the method of Cain - Bohmann modified yielding presence of good amount of saponins, which were identified as triterpenoid saponins using qualitative tests that were positive and the test of the foam reaction with the reagent Salwosky, Bouch...

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Detalles Bibliográficos
Autores: Flores, T., Huamán, J. Huamán, Tomás, G.
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2013
País:Perú
Institución:Universidad Nacional Mayor de San Marcos
Repositorio:Revistas - Universidad Nacional Mayor de San Marcos
Idioma:español
OAI Identifier:oai:revistasinvestigacion.unmsm.edu.pe:article/6532
Acceso en línea:https://revistasinvestigacion.unmsm.edu.pe/index.php/quim/article/view/6532
Access Level:acceso abierto
Palabra clave:saponins
triterpenes
detergency
aglycones
hydrolysi
saponinas
triterpenos
detergencia
agliconas
hidrólisis
Descripción
Sumario:In our research, a phytochemical screening was performed by the method of Cain - Bohmann modified yielding presence of good amount of saponins, which were identified as triterpenoid saponins using qualitative tests that were positive and the test of the foam reaction with the reagent Salwosky, Bouchard Liberman reagent and reaction with sulfuric acid. Three quantitative methods for extracting saponins from a hydroalcoholic extract of the plant and subsequent hydrolysis were developed. The difference of the first two methods was to use a method with the sample defatted with chloroform and the other without scouring . For the third method according to the procedure applied M.E.Wall et al. (1958). Extraction rates for the three methods saponins were 3.90%, 2.40 % and 2.02% respectively. Similarly the corresponding aglycones after acid were obtained by hydrolyzing the crude obtained via.