Catalytic Activity of Rhodium (I) Complexes with Bidentate Phosphinic Ligands in the Hydrogenation of Unsaturated Alycyclic Substrates

RhCl(dppe)2, RhCl(dppp)2 and RhCl(dppb)2, where dppe =diphenylphosphinoethane; dppp = diphenylphosphinopropane; dppb= diphenylphosphinobutane complexes were prepared by treatingRhCl3.3H2O with the appropriate di(tertiaryphosphine). These complexeswere used as catalytic precursors in the hydrogenatio...

Descripción completa

Detalles Bibliográficos
Autores: Liliana Montalvo, Alberto Bolaños, Armando Cabrera
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2007
País:México
Institución:Universidad Nacional Autónoma de México
Repositorio:Redalyc-UNAM
OAI Identifier:oai:redalyc.org:47551103
Acceso en línea:https://www.redalyc.org/articulo.oa?id=47551103
Access Level:acceso abierto
Palabra clave:Química
Rhodium
homogeneous catalysis
catalytic hydrogenation
bidentate phosphinic ligands
unsaturated alycyclic compounds
Descripción
Sumario:RhCl(dppe)2, RhCl(dppp)2 and RhCl(dppb)2, where dppe =diphenylphosphinoethane; dppp = diphenylphosphinopropane; dppb= diphenylphosphinobutane complexes were prepared by treatingRhCl3.3H2O with the appropriate di(tertiaryphosphine). These complexeswere used as catalytic precursors in the hydrogenation oflimonene, camphene and 1,5- cyclooctadiene at different concentrationsand temperatures. It was found that the Rhodium complex havingdppp as ligand was the best catalytic precursor.