Dimeric Boronates Derived from the Reaction of Schiff Bases and Boronic Acids

The one-pot synthesis of dimeric boron complexes is reported. The compounds were obtainedby reaction of Schiff bases (tridentate ligands) with trans-β-phenylvinylboronic acid, 3-thiopheneboronic acid and methylboronic acid. Building of the dimeric structures is favored by thepresence of int...

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Detalles Bibliográficos
Autores: Victor Barba, Rosa Santillan, Norberto Farfán
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2005
País:México
Institución:Universidad Autónoma del Estado de Morelos
Repositorio:Redalyc-UAEM
OAI Identifier:oai:redalyc.org:47549220
Acceso en línea:https://www.redalyc.org/articulo.oa?id=47549220
Access Level:acceso abierto
Palabra clave:Química
boron
Schiff base
macrocyclic chem
tridentate ligands
Descripción
Sumario:The one-pot synthesis of dimeric boron complexes is reported. The compounds were obtainedby reaction of Schiff bases (tridentate ligands) with trans-β-phenylvinylboronic acid, 3-thiopheneboronic acid and methylboronic acid. Building of the dimeric structures is favored by thepresence of intramolecular N→B coordination bonds, resulting in the formation of ten-memberedring heterocycles. An X-ray crystallographic analysis for one of them confirmed the dimeric natureof these compounds.