Influence of the Si/Al framework ratio on the microporosity of dealuminated mordenite as determined from N-2 adsorption

Dealuminated mordenites depicting SiO2/Al2O3 molar ratios in the range 10-206 were analyzed through adsorption methods. The Type I-IV hybrid shape of the N-2 adsorption isotherms at 76 K on dealuminated mordenites indicated rather high micropore contents, though some amount of mesopores of slit-like...

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Detalhes bibliográficos
Autores: Petranovskii, V, Portillo, R, Rojas, F, Lara, VH, Hernández, MA, Avalos, MA
Tipo de documento: artigo
Estado:Versão publicada
Data de publicação:2006
País:México
Recursos:Universidad Nacional Autónoma de México
Repositório:Sistema de Información de la Facultad de Ciencias, UNAM
OAI Identifier:oai:repositorio.fciencias.unam.mx:11154/1304
Acesso em linha:http://hdl.handle.net/11154/1304
Access Level:Acceso aberto
Palavra-chave:Chemistry, Multidisciplinary
Engineering, Chemical
dealuminated mordenite
high-resolution alpha s plots
supermicropores
ultramicropores
Dubinin-Astakhov
Descrição
Resumo:Dealuminated mordenites depicting SiO2/Al2O3 molar ratios in the range 10-206 were analyzed through adsorption methods. The Type I-IV hybrid shape of the N-2 adsorption isotherms at 76 K on dealuminated mordenites indicated rather high micropore contents, though some amount of mesopores of slit-like geometry was also present. Micropore volumes and sizes were measured through alpha(S) , t , and DA-plots, as well as by the NLDFT approach. Results indicated that mordenite dealumination caused micropore opening and widening as well as the emergence of further slit-like mesopores