Side-Wall Functionalization of Multi-Walled Carbon Nanotubes with t-Butyl Diazoacetate

The covalent functionalization of multiwall carbon nanotubes (MWCNT) and its characterization techniques are reported. MWCNT were functionalized with tert-butyldiazoacetate to give methano-bridged ester group. Functionalized carbon nanotube by ester and its hydrolyzed carboxylic acid were characteri...

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Detalhes bibliográficos
Autores: Eduardo Rogel-Hernández, Gabriel Alonso-Nuñez, Juan P. Camarena, Heriberto Espinoza-Gómez, Gerardo Aguirre, Francisco Paraguay-Delgado, Ratnasamy Somanathan
Tipo de documento: artigo
Estado:Versão publicada
Data de publicação:2011
País:México
Recursos:Universidad Nacional Autónoma de México
Repositório:Redalyc-UNAM
OAI Identifier:oai:redalyc.org:47521267003
Acesso em linha:https://www.redalyc.org/articulo.oa?id=47521267003
Access Level:Acceso aberto
Palavra-chave:Química
multi
ester
Multi
methano
bridged ester
Descrição
Resumo:The covalent functionalization of multiwall carbon nanotubes (MWCNT) and its characterization techniques are reported. MWCNT were functionalized with tert-butyldiazoacetate to give methano-bridged ester group. Functionalized carbon nanotube by ester and its hydrolyzed carboxylic acid were characterized by high resolution electron microscope techniques, scanning electron microscopy (SEM), transmission electron microscopy (TEM) to study the shape a structure and fast Fourier transform infrared (FT-IR) to evaluate types of binding.