Synthesis and characterization of new 2-(alkylamino) acetamides
Seven new 2-(alkylamino) acetamides have been synthesized and characterized by 1H, 13C NMR, NOESY experiments, infrared and mass spectrometry. The structure of 2-(diphenylmethylamino) acetamide 3b was further established by a single crystal x-ray diffraction study. The NMR study of the transformatio...
| Authors: | , |
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| Format: | article |
| Status: | Published version |
| Publication Date: | 2003 |
| Country: | México |
| Institution: | Universidad Autónoma Metropolitana |
| Repository: | Concentración de Recursos de Información Científica y Académica, UAM Cuajimalpa |
| Language: | English |
| OAI Identifier: | oai:ilitia.cua.uam.mx:123456789/57 |
| Online Access: | http://ilitia.cua.uam.mx:8080/jspui/handle/123456789/57 |
| Access Level: | Open access |
| Keyword: | info:eu-repo/classification/cti/2 Acetamidas Amidas Espectroscopia Rayos X |
| Summary: | Seven new 2-(alkylamino) acetamides have been synthesized and characterized by 1H, 13C NMR, NOESY experiments, infrared and mass spectrometry. The structure of 2-(diphenylmethylamino) acetamide 3b was further established by a single crystal x-ray diffraction study. The NMR study of the transformation of several 2-(alkylamino) acetamides to their corresponding morpholin-2-ones shows that these species are thermodynamically favored through preferred conformations as determined by theoretical calculations of 3h. |
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