Impact of Physicochemical Parameters on In Vitro Assembly and Disassembly Kinetics of Recombinant Triple-Layered Rotavirus-Like Particles

Virus-like particles constitute potentially relevant vaccine candidates. Nevertheless, their behavior in vitro and assembly process needs to be understood in order to improve their yield and quality. In this study we aimed at addressing these issues and for that purpose triple- and double-layered ro...

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Detalles Bibliográficos
Autores: Mellado, MCM, Mena, JA, Lopes, A, Ramirez, OT, Carrondo, MJT, Palomares, LA, Alves, PM
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2009
País:México
Institución:Universidad Nacional Autónoma de México
Repositorio:Sistema de Información de la Facultad de Ciencias, UNAM
OAI Identifier:oai:repositorio.fciencias.unam.mx:11154/2192
Acceso en línea:http://hdl.handle.net/11154/2192
Access Level:acceso abierto
Palabra clave:Biotechnology & Applied Microbiology
rotavirus-like particles
disassembly kinetics
assembly kinetics
light scattering
capillary zone electrophoresis
Descripción
Sumario:Virus-like particles constitute potentially relevant vaccine candidates. Nevertheless, their behavior in vitro and assembly process needs to be understood in order to improve their yield and quality. In this study we aimed at addressing these issues and for that purpose triple- and double-layered rotavirus-like particles (TLP 2/6/7 and DLP 2/6, respectively) size and zeta potential were measured using dynamic light scattering at different physicochemical conditions, namely pH, ionic strength,. and temperature. Both TLP and DLP were stable within a PH range of 3-7 and at 5-25 degrees C. Aggregation occurred at 35-45 degrees C and their disassembly became evident at 65 degrees C. The isoelectric points of TLP and DLP were 3.0 and 3.8, respectively. In vitro kinetics of TLP disassembly was monitored. Ionic strength, temperature, and the chelating agent employed determined disassembly kinetics. Glycerol (10%) stabilized TLP by preventing its disassembly. Disassembled TLP was able to reassemble by dialysis at high calcium conditions. VP7 monomers were added to DLP in the presence of calcium to follow in vitro TLP assembly kinetics