Electrochemical performance of YSZ coupled Ba_(0.5)Sr_(0.5)Fe_(0.9)Cu_(0.1)O_(3-δ) electrode at intermediate temperature

Abstract. Synthesis of electrolyte 8% Y2O3 Stabilized Zirconia (YSZ) and characterization of electrical conductivity with BSFC Ba0.5Sr0.5Fe0.9Cu0.1O3-δ (BSFC) electrode have been conducted. YSZ and BSFC were synthesized using sol-gel self-combustion. YSZ powder was calcined at 700℃ for 2 hours, then...

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Autores: Setiyono, S., Fitriana, F., Baqiya, M. A., Suasmoro, S.
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2024
País:México
Institución:UNIVERSIDAD NACIONAL AUTÓNOMA DE MÉXICO
Repositorio:Journal of Applied Research and Technology
Idioma:inglés
OAI Identifier:oai:ojs2.localhost:article/2331
Acceso en línea:https://jart.icat.unam.mx/index.php/jart/article/view/2331
Access Level:acceso abierto
Palabra clave:Cole-Cole plot
Debye relaxation
electrolyte YSZ
electrode
impedance
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spelling Electrochemical performance of YSZ coupled Ba_(0.5)Sr_(0.5)Fe_(0.9)Cu_(0.1)O_(3-δ) electrode at intermediate temperatureSetiyono, S.Fitriana, F.Baqiya, M. A.Suasmoro, S.Cole-Cole plotDebye relaxation electrolyte YSZelectrodeimpedanceAbstract. Synthesis of electrolyte 8% Y2O3 Stabilized Zirconia (YSZ) and characterization of electrical conductivity with BSFC Ba0.5Sr0.5Fe0.9Cu0.1O3-δ (BSFC) electrode have been conducted. YSZ and BSFC were synthesized using sol-gel self-combustion. YSZ powder was calcined at 700℃ for 2 hours, then pressed into a disk and sintered at 1550 ⁰C for 6 hours. While BSFC powder was calcined at 850 ℃ for 6 hours and sintered at 1100 ⁰C for 6 hours. X-ray diffraction (XRD) analysis shows that calcined powder of both YSZ and BSFC has cubic structure possessing space group (Fm-3m) and (Pm-3m), respectively. The lattice parameter of the YSZ a = 5.17 Å and the crystallite size Φ ≈ 11 nm were evaluated using the Debye-Scherer equation.  A scanning electron microscope (SEM) shows that BSFC can adhere well to the surface of YSZ. The electrical behavior of the YSZ and half-cell BSFC||YSZ||BSFC measured at 150- 850 ⁰C shows the resistivity decreased with increasing temperature. The resistivity of BSFC||YSZ||BSFC is lower than YSZ due to the influence of BSFC. Cathode material BSFC is suitable for YSZ electrolytes.Universidad Nacional Autónoma de México2024-06-28info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionPeer-reviewed Articleapplication/pdfhttps://jart.icat.unam.mx/index.php/jart/article/view/233110.22201/icat.24486736e.2024.22.3.2331Journal of Applied Research and Technology; Vol. 22 No. 3 (2024); 410-418Journal of Applied Research and Technology; Vol. 22 Núm. 3 (2024); 410-4182448-67361665-6423reponame:Journal of Applied Research and Technologyinstname:UNIVERSIDAD NACIONAL AUTÓNOMA DE MÉXICOinstacron:UNAMenghttps://jart.icat.unam.mx/index.php/jart/article/view/2331/1115Copyright (c) 2024 Universidad Nacional Autónoma de Méxicohttp://creativecommons.org/licenses/by-nc-nd/4.0info:eu-repo/semantics/openAccessoai:ojs2.localhost:article/23312024-08-16T17:54:21Z
dc.title.none.fl_str_mv Electrochemical performance of YSZ coupled Ba_(0.5)Sr_(0.5)Fe_(0.9)Cu_(0.1)O_(3-δ) electrode at intermediate temperature
title Electrochemical performance of YSZ coupled Ba_(0.5)Sr_(0.5)Fe_(0.9)Cu_(0.1)O_(3-δ) electrode at intermediate temperature
spellingShingle Electrochemical performance of YSZ coupled Ba_(0.5)Sr_(0.5)Fe_(0.9)Cu_(0.1)O_(3-δ) electrode at intermediate temperature
Setiyono, S.
Cole-Cole plot
Debye relaxation
electrolyte YSZ
electrode
impedance
title_short Electrochemical performance of YSZ coupled Ba_(0.5)Sr_(0.5)Fe_(0.9)Cu_(0.1)O_(3-δ) electrode at intermediate temperature
title_full Electrochemical performance of YSZ coupled Ba_(0.5)Sr_(0.5)Fe_(0.9)Cu_(0.1)O_(3-δ) electrode at intermediate temperature
title_fullStr Electrochemical performance of YSZ coupled Ba_(0.5)Sr_(0.5)Fe_(0.9)Cu_(0.1)O_(3-δ) electrode at intermediate temperature
title_full_unstemmed Electrochemical performance of YSZ coupled Ba_(0.5)Sr_(0.5)Fe_(0.9)Cu_(0.1)O_(3-δ) electrode at intermediate temperature
title_sort Electrochemical performance of YSZ coupled Ba_(0.5)Sr_(0.5)Fe_(0.9)Cu_(0.1)O_(3-δ) electrode at intermediate temperature
dc.creator.none.fl_str_mv Setiyono, S.
Fitriana, F.
Baqiya, M. A.
Suasmoro, S.
author Setiyono, S.
author_facet Setiyono, S.
Fitriana, F.
Baqiya, M. A.
Suasmoro, S.
author_role author
author2 Fitriana, F.
Baqiya, M. A.
Suasmoro, S.
author2_role author
author
author
dc.subject.none.fl_str_mv Cole-Cole plot
Debye relaxation
electrolyte YSZ
electrode
impedance
topic Cole-Cole plot
Debye relaxation
electrolyte YSZ
electrode
impedance
description Abstract. Synthesis of electrolyte 8% Y2O3 Stabilized Zirconia (YSZ) and characterization of electrical conductivity with BSFC Ba0.5Sr0.5Fe0.9Cu0.1O3-δ (BSFC) electrode have been conducted. YSZ and BSFC were synthesized using sol-gel self-combustion. YSZ powder was calcined at 700℃ for 2 hours, then pressed into a disk and sintered at 1550 ⁰C for 6 hours. While BSFC powder was calcined at 850 ℃ for 6 hours and sintered at 1100 ⁰C for 6 hours. X-ray diffraction (XRD) analysis shows that calcined powder of both YSZ and BSFC has cubic structure possessing space group (Fm-3m) and (Pm-3m), respectively. The lattice parameter of the YSZ a = 5.17 Å and the crystallite size Φ ≈ 11 nm were evaluated using the Debye-Scherer equation.  A scanning electron microscope (SEM) shows that BSFC can adhere well to the surface of YSZ. The electrical behavior of the YSZ and half-cell BSFC||YSZ||BSFC measured at 150- 850 ⁰C shows the resistivity decreased with increasing temperature. The resistivity of BSFC||YSZ||BSFC is lower than YSZ due to the influence of BSFC. Cathode material BSFC is suitable for YSZ electrolytes.
publishDate 2024
dc.date.none.fl_str_mv 2024-06-28
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
Peer-reviewed Article
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv https://jart.icat.unam.mx/index.php/jart/article/view/2331
10.22201/icat.24486736e.2024.22.3.2331
url https://jart.icat.unam.mx/index.php/jart/article/view/2331
identifier_str_mv 10.22201/icat.24486736e.2024.22.3.2331
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv https://jart.icat.unam.mx/index.php/jart/article/view/2331/1115
dc.rights.none.fl_str_mv Copyright (c) 2024 Universidad Nacional Autónoma de México
http://creativecommons.org/licenses/by-nc-nd/4.0
info:eu-repo/semantics/openAccess
rights_invalid_str_mv Copyright (c) 2024 Universidad Nacional Autónoma de México
http://creativecommons.org/licenses/by-nc-nd/4.0
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
dc.publisher.none.fl_str_mv Universidad Nacional Autónoma de México
publisher.none.fl_str_mv Universidad Nacional Autónoma de México
dc.source.none.fl_str_mv Journal of Applied Research and Technology; Vol. 22 No. 3 (2024); 410-418
Journal of Applied Research and Technology; Vol. 22 Núm. 3 (2024); 410-418
2448-6736
1665-6423
reponame:Journal of Applied Research and Technology
instname:UNIVERSIDAD NACIONAL AUTÓNOMA DE MÉXICO
instacron:UNAM
instname_str UNIVERSIDAD NACIONAL AUTÓNOMA DE MÉXICO
instacron_str UNAM
institution UNAM
reponame_str Journal of Applied Research and Technology
collection Journal of Applied Research and Technology
repository.name.fl_str_mv
repository.mail.fl_str_mv
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