Structure and characterization of hot dip galvanized coatings in acidic medium in low carbon steel.

In the present work, the structural and microstructural characterization and mechanical properties analysis of hot-dip galvanized coatings on steel sheets was carried out, sometimes at different temperatures of a liquid Zn bath and different immersion times, with the intention to determine the ideal...

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Detalles Bibliográficos
Autores: Ruiz, Milton, Hernández-Ávila, Juan, Cerecedo-Sáenz, Eduardo, Salinas-Rodríguez, Eleazar, López-García, Ricardo D., Maldonado-Reyes, Aracely, Mexicano-Santoyo, Adriana
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2020
País:México
Institución:UNIVERSIDAD AUTÓNOMA DEL ESTADO DE HIDALGO
Repositorio:PÄDI Boletín Científico de Ciencias Básicas e Ingeniería del ICBI
Idioma:español
OAI Identifier:oai:repository.uaeh.edu.mx:article/5701
Acceso en línea:https://repository.uaeh.edu.mx/revistas/index.php/icbi/article/view/5701
Access Level:acceso abierto
Palabra clave:GALVANIZED
HOT DIP
CRYSTAL STRUCTURE
DRX
MEB
GALVANIZADO
INMERSION EN CALIENTE
ESTRUCTURA CRISTALINA
Descripción
Sumario:In the present work, the structural and microstructural characterization and mechanical properties analysis of hot-dip galvanized coatings on steel sheets was carried out, sometimes at different temperatures of a liquid Zn bath and different immersion times, with the intention to determine the ideal conditions of adherence and mechanical properties. Cleaning of the low-content steel sheets was carried out using a 1 M concentration of HCL. Likewise, an instrumental analysis was performed by X-ray diffraction (XRD), Zn was identified with PDF [96-230-0115] BCC with 4.51% crystallinity and 1Å of crystallite size, and PDF [96-901- 0309] FCC with 21.21% crystallinity and 2Å; Jarosite was identified which shows that an immersion in an acid medium causes a hydrolysis of iron and extraction of phosphorus and sulfur from the steel matrix. Furthermore, by scanning electron microscopy (MEB-EDS), the size of the coating layers of the compounds formed on these layers was determined. From what is concluded, that the cleaning with HCL after sandblast cleaning and a hot dip galvanizing temperature of 473 ° C, one minute of heating the sheet before immersion and two minutes of immersion in the liquid bath Zn are the best conditions for a good adhesion of coating on a steel coating.