MORPHOMETRIC CHARACTERIZATION OF SPRAY-DRIED MICROCAPSULES BEFORE AND AFTER -TOCOPHEROL EXTRACTION

Microcapsules were obtained by spray-drying of -tocopherol (AT) - in- water emulsions subjected to single and double atomization yielding single atomized microcapsules (SAM) and double atomized microcapsules (DAM) which had di erent core to wall material ratios. Micrographs of whole and AT extracted...

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Detalles Bibliográficos
Autores: M.X. Quintanilla-Carvajal, L.S. Meraz-Torres, L. Alamilla-Beltrán, J.J. Chanona-Pérez, E. Terres-Rojas, H. Hernández-Sánchez, A.R. Jiménez-Aparicio, G.F. Gutiérrez-López
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2011
País:México
Institución:Instituto Mexicano del Petróleo
Repositorio:Redalyc-IMP
OAI Identifier:oai:redalyc.org:62020825013
Acceso en línea:https://www.redalyc.org/articulo.oa?id=62020825013
Access Level:acceso abierto
Palabra clave:Ingeniería
spray drying
image analysis
alpha tocopherol
Morphometric parameters
Descripción
Sumario:Microcapsules were obtained by spray-drying of -tocopherol (AT) - in- water emulsions subjected to single and double atomization yielding single atomized microcapsules (SAM) and double atomized microcapsules (DAM) which had di erent core to wall material ratios. Micrographs of whole and AT extracted of SAM and DAM obtained from Environmental Scanning Electron Microscopy (ESEM) were image analyzed and the Feret diameter, projected area, perimeter, maximum perimeter, shape factor and Fractal Dimension of contour (FDc) and texture (FDt) were determined. Whole DAM presented higher FDc and FDt than SAM, while SAM presented higher FDc values for all the microcapsules and higher DFt values for the AT to wall materials ratios 1:4 after the AT extraction. Most of the microcapsules displayed significantly di erent perimeter but non- significant projected areas, whereas the extracted microcapsules tended not to show significant di erences between these two parameters.