Determination of the surface functionality of nanocarbon allotropes by boehm titration
Critical point (CP) in a titration curve to quantify carboxylic, lactonic, and phenolic groups on multi-walled carbon nanotube (CNT) and Vulcan carbon (VC). Titration technique used was Boehm type and tipping point measurement from titration curve was done by second derivative method. The calculatio...
| Autores: | , , , , , , , , , |
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| Tipo de recurso: | artículo |
| Estado: | Versión publicada |
| Fecha de publicación: | 2020 |
| País: | México |
| Institución: | Universidad Autónoma de Zacatecas |
| Repositorio: | Repositorio Institucional Caxcán |
| Idioma: | español |
| OAI Identifier: | oai:http://ricaxcan.uaz.edu.mx:20.500.11845/2543 |
| Acceso en línea: | http://ricaxcan.uaz.edu.mx/jspui/handle/20.500.11845/2543 |
| Access Level: | acceso abierto |
| Palabra clave: | BIOLOGIA Y QUIMICA [2] Surface functionality nanocarbons Boehm titration |
| Sumario: | Critical point (CP) in a titration curve to quantify carboxylic, lactonic, and phenolic groups on multi-walled carbon nanotube (CNT) and Vulcan carbon (VC). Titration technique used was Boehm type and tipping point measurement from titration curve was done by second derivative method. The calculation functional groups on nanocarbons (NCs) presents lowest uncertainty previously published. An order of ±10−4meq/g is the precision of the values obtained, one order of magnitude below reported. Both NCs display a high quantity of carboxylic groups created after being treated with regard to the other functional groups generated, mainly for functionalized Vulcan carbon VC-F. |
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