Determination of Polyethylene Glycols in Water by Reversed-Phase High-Performance Liquid Chromatography

This paper describes an RP-HPLC method to characterize the ozonation products of polyethylene glycols (PEGs) (general formula HO(CH 2CH 2O) n -H) with original mass 5000. Samples with different pH and ozonation times were studied. The amounts of individual products up to n = 56, the percentage of PE...

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Detalhes bibliográficos
Autores: Moldovan, Z, Delgado Luque, M.V, Otal Salaverri, Emilia, Suárez, Ana, Andreozzi, R, Insola, A, Lebrato Martínez, Julián
Tipo de documento: artigo
Estado:Versión aceptada para publicación
Data de publicação:1996
País:España
Recursos:Universidad de Sevilla (US)
Repositório:idUS. Depósito de Investigación de la Universidad de Sevilla
OAI Identifier:oai:idus.us.es:11441/49579
Acesso em linha:http://hdl.handle.net/11441/49579
Access Level:Acceso aberto
Palavra-chave:Ozonation
Polyethylene glycols
Descrição
Resumo:This paper describes an RP-HPLC method to characterize the ozonation products of polyethylene glycols (PEGs) (general formula HO(CH 2CH 2O) n -H) with original mass 5000. Samples with different pH and ozonation times were studied. The amounts of individual products up to n = 56, the percentage of PEGs as a final product and the molecular distribution ( M w/ M n) were calculated. The samples were concentrated by liquid-liquid extraction.