Topical meloxicam hydroxipropyl guar hydrogels based on low-substituted hydroxypropyl cellulose solid dispersions

Meloxicam (MX) is a poorly water-soluble drug with severe gastrointestinal side effects. Topical hydrogel of hydroxypropyl guar (HPG) was formulated using a solid dispersion (SD) of MX with hydroxypropyl cellulose (LHPC) as an alternative to oral administration. The development of a solid dispersion...

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Detalles Bibliográficos
Autores: Dahma, Zaid, Torrado Salmerón, Carlos Félix, Álvarez Álvarez, Covandonga, Guarnizo Herrero, Víctor|||0000-0001-9323-3388, Martínez Alonso, Borja, Torrado Durán, Guillermo|||0000-0002-8865-2083, Torrado Durán, Santiago, Torre Iglesias, Paloma de la
Tipo de recurso: artículo
Fecha de publicación:2024
País:España
Institución:Universidad de Alcalá (UAH)
Repositorio:e_Buah Biblioteca Digital Universidad de Alcalá
Idioma:inglés
OAI Identifier:oai:ebuah.uah.es:10017/66155
Acceso en línea:http://hdl.handle.net/10017/66155
https://dx.doi.org/10.3390/gels10030207
Access Level:acceso abierto
Palabra clave:Meloxicam
Low-substituted hydroxypropyl cellulose
Hydroxypropyl guar
Solid dispersion
Hydrogels
Polymer/polymer interactions
Farmacia
Pharmacy
Descripción
Sumario:Meloxicam (MX) is a poorly water-soluble drug with severe gastrointestinal side effects. Topical hydrogel of hydroxypropyl guar (HPG) was formulated using a solid dispersion (SD) of MX with hydroxypropyl cellulose (LHPC) as an alternative to oral administration. The development of a solid dispersion with an adequate MX:LHPC ratio could increase the topical delivery of meloxicam. Solid dispersions showed high MX solubility values and were related to an increase in hydrophilicity. The drug/polymer and polymer/polymer interactions of solid dispersions within the HPG hydrogels were evaluated by SEM, DSC, FTIR, and viscosity studies. A porous structure was observed in the solid dispersion hydrogel MX:LHPC (1:2.5) and its higher viscosity was related to a high increase in hydrogen bonds among the –OH groups from LHPC and HPG with water molecules. In vitro drug release studies showed increases of 3.20 and 3.97-fold for hydrogels with MX:LHPC ratios of (1:1) and (1:2.5), respectively, at 2 h compared to hydrogel with pure MX. Finally, a fitting transition from zero to first-order model was observed for these hydrogels containing solid dispersions, while the n value of Korsmeyer–Peppas model indicated that release mechanism is governed by diffusion through an important relaxation of the polymer.