A novel class of multitarget anti-Alzheimer benzohomoadamantane‒chlorotacrine hybrids modulating cholinesterases and glutamate NMDA receptors

The development of multitarget compounds against multifactorial diseases, such as Alzheimer's disease, is an area of very intensive research, due to the expected superior therapeutic efficacy that should arise from the simultaneous modulation of several key targets of the complex pathological n...

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Bibliographic Details
Authors: Pérez Areales, Francisco Javier, Turcu, Andreea L., Barniol-Xicota, Marta, Pont Masanet, Caterina, Pivetta, Deborah, Espargaró Colomé, Alba, Bartolini, Manuela, De Simone, Angela, Andrisano, Vincenza, Pérez, Belén, Sabaté Lagunas, Raimon, Sureda, Francesc X., Vázquez Cruz, Santiago, Muñoz-Torrero López-Ibarra, Diego
Format: article
Status:Versión aceptada para publicación
Publication Date:2019
Country:España
Institution:Varias* (Consorci de Biblioteques Universitáries de Catalunya, Centre de Serveis Científics i Acadèmics de Catalunya)
Repository:Recercat. Dipósit de la Recerca de Catalunya
OAI Identifier:oai:recercat.cat:2445/141878
Online Access:https://hdl.handle.net/2445/141878
Access Level:Open access
Keyword:Malaltia d'Alzheimer
Malalties neurodegeneratives
Escorça cerebral
Química farmacèutica
Alzheimer's disease
Neurodegenerative Diseases
Cerebral cortex
Pharmaceutical chemistry
Description
Summary:The development of multitarget compounds against multifactorial diseases, such as Alzheimer's disease, is an area of very intensive research, due to the expected superior therapeutic efficacy that should arise from the simultaneous modulation of several key targets of the complex pathological network. Here we describe the synthesis and multitarget biological profiling of a new class of compounds designed by molecular hybridization of an NMDA receptor antagonist fluorobenzohomoadamantanamine with the potent acetylcholinesterase (AChE) inhibitor 6-chlorotacrine, using two different linker lengths and linkage positions, to preserve or not the memantine-like polycyclic unsubstituted primary amine. The best hybrids exhibit greater potencies than parent compounds against AChE (IC50 0.33 nM in the best case, 44-fold increased potency over 6-chlorotacrine), butyrylcholinesterase (IC50 21 nM in the best case, 24-fold increased potency over 6-chlorotacrine), and NMDA receptors (IC50 0.89 µM in the best case, 2-fold increased potency over the parent benzohomoadamantanamine and memantine), which suggests an additive effect of both pharmacophoric moieties in the interaction with the primary targets. Moreover, most of these compounds have been predicted to be brain permeable. This set of biological properties makes them promising leads for further anti-Alzheimer drug development.