Hybrid nonlinear autoregressive neural network—Weibull statistical model applied to the supercritical extraction of lanolin from raw wool

Supercritical extraction of lanolin from raw wool with modified CO2 (5% ethanol) at temperatures above the melting point of lanolin (T = 36–42 ºC) is difficult to model because of the multicomponent diffusion in the liquid layer. In this work, a neural network model is proposed based on the experime...

Descripción completa

Detalles Bibliográficos
Autores: Valverde Salamanca, Abel|||0000-0002-0179-117X, Álvarez Flórez, Jesús Andrés|||0000-0002-0909-0087, Recasens Baxarías, Francisco Javier
Tipo de recurso: artículo
Fecha de publicación:2020
País:España
Institución:Universitat Politècnica de Catalunya (UPC)
Repositorio:UPCommons. Portal del coneixement obert de la UPC
Idioma:inglés
OAI Identifier:oai:upcommons.upc.edu:2117/330068
Acceso en línea:https://hdl.handle.net/2117/330068
https://dx.doi.org/10.1007/s42452-020-03475-7
Access Level:acceso abierto
Palabra clave:Lanolin
Wool-fat
Neural networks (Neurobiology)
Genetic algorithms
High pressure extraction
Neural networks
Genetic algorithm
Weibull
Lanolina
Llana--Greix
Xarxes neuronals (Neurobiologia)
Algorismes genètics
Àrees temàtiques de la UPC::Enginyeria química
Descripción
Sumario:Supercritical extraction of lanolin from raw wool with modified CO2 (5% ethanol) at temperatures above the melting point of lanolin (T = 36–42 ºC) is difficult to model because of the multicomponent diffusion in the liquid layer. In this work, a neural network model is proposed based on the experiments previously published by our research group. Experimentally, the extraction of a 100-cm3 packed bed of raw wool depends on five variables, i.e., temperature (60–80 ºC), pressure (120–200 bar), solvent mass flow rate (3–5 kg/h), wool packing density (127–318 kg/m3), and time (~ 1 h). A nonlinear autoregressive exogenous (5,3,1) neural network was designed and trained with the experimental data aug-mented using an empirical Weibull statistical function. This correctly predicts the lanolin breakthrough at the extractor exit with only ± 0.42% error. The simple arithmetics of neural network allows a fast optimization with Genetic Algorithm to find optimum operation conditions for the extraction process