Characterisation and determination of fullerenes: a critical review

A prominent sector of nanotechnology is occupied by a class of carbon-based nanoparticles known as fullerenes. Fullerene particle size and shape impact in how easily these particles are transported into and throughout the environment and living tissues. Currently, there is a lack of adequate methodo...

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Detalhes bibliográficos
Autores: Astefanei, Alina, Núñez Burcio, Oscar, Galcerán Huguet, M. Teresa
Formato: artículo
Estado:Versión aceptada para publicación
Fecha de publicación:2015
País:España
Recursos:Varias* (Consorci de Biblioteques Universitáries de Catalunya, Centre de Serveis Científics i Acadèmics de Catalunya)
Repositorio:Recercat. Dipósit de la Recerca de Catalunya
OAI Identifier:oai:recercat.cat:2445/66853
Acesso em linha:https://hdl.handle.net/2445/66853
Access Level:acceso abierto
Palavra-chave:Ful·lerens
Fullerenes
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spelling Characterisation and determination of fullerenes: a critical reviewAstefanei, AlinaNúñez Burcio, OscarGalcerán Huguet, M. TeresaFul·lerensFullerenesA prominent sector of nanotechnology is occupied by a class of carbon-based nanoparticles known as fullerenes. Fullerene particle size and shape impact in how easily these particles are transported into and throughout the environment and living tissues. Currently, there is a lack of adequate methodology for their size and shape characterisation, identification and quantitative detection in environmental and biological samples. The most commonly used methods for their size measurements (aggregation, size distribution, shape, etc.), the effect of sampling and sample treatment on these characteristics and the analytical methods proposed for their determination in complex matrices are discussed in this review. For the characterisation and analysis of fullerenes in real samples, different analytical techniques including microscopy, spectroscopy, flow field-flow fractionation, electrophoresis, light scattering, liquid chromatography and mass spectrometry have been reported. The existing limitations and knowledge gaps in the use of these techniques are discussed and the necessity to hyphenate complementary ones for the accurate characterisation, identification and quantitation of these nanoparticles is highlighted.Elsevier B.V.2015201520152015info:eu-repo/semantics/articleinfo:eu-repo/semantics/acceptedVersion69 p.application/pdfhttps://hdl.handle.net/2445/66853Articles publicats en revistes (Enginyeria Química i Química Analítica)reponame:Recercat. Dipósit de la Recerca de Catalunyainstname:Varias* (Consorci de Biblioteques Universitáries de Catalunya, Centre de Serveis Científics i Acadèmics de Catalunya)InglésVersió postprint del document publicat a: http://dx.doi.org/10.1016/j.aca.2015.03.025Analytica Chimica Acta, 2015, vol. 882, p. 1-21http://dx.doi.org/10.1016/j.aca.2015.03.025cc-by-nc-nd (c) Elsevier B.V., 2015http://creativecommons.org/licenses/by-nc-nd/3.0/esinfo:eu-repo/semantics/openAccessoai:recercat.cat:2445/668532026-05-29T05:05:01Z
dc.title.none.fl_str_mv Characterisation and determination of fullerenes: a critical review
title Characterisation and determination of fullerenes: a critical review
spellingShingle Characterisation and determination of fullerenes: a critical review
Astefanei, Alina
Ful·lerens
Fullerenes
title_short Characterisation and determination of fullerenes: a critical review
title_full Characterisation and determination of fullerenes: a critical review
title_fullStr Characterisation and determination of fullerenes: a critical review
title_full_unstemmed Characterisation and determination of fullerenes: a critical review
title_sort Characterisation and determination of fullerenes: a critical review
dc.creator.none.fl_str_mv Astefanei, Alina
Núñez Burcio, Oscar
Galcerán Huguet, M. Teresa
author Astefanei, Alina
author_facet Astefanei, Alina
Núñez Burcio, Oscar
Galcerán Huguet, M. Teresa
author_role author
author2 Núñez Burcio, Oscar
Galcerán Huguet, M. Teresa
author2_role author
author
dc.subject.none.fl_str_mv Ful·lerens
Fullerenes
topic Ful·lerens
Fullerenes
description A prominent sector of nanotechnology is occupied by a class of carbon-based nanoparticles known as fullerenes. Fullerene particle size and shape impact in how easily these particles are transported into and throughout the environment and living tissues. Currently, there is a lack of adequate methodology for their size and shape characterisation, identification and quantitative detection in environmental and biological samples. The most commonly used methods for their size measurements (aggregation, size distribution, shape, etc.), the effect of sampling and sample treatment on these characteristics and the analytical methods proposed for their determination in complex matrices are discussed in this review. For the characterisation and analysis of fullerenes in real samples, different analytical techniques including microscopy, spectroscopy, flow field-flow fractionation, electrophoresis, light scattering, liquid chromatography and mass spectrometry have been reported. The existing limitations and knowledge gaps in the use of these techniques are discussed and the necessity to hyphenate complementary ones for the accurate characterisation, identification and quantitation of these nanoparticles is highlighted.
publishDate 2015
dc.date.none.fl_str_mv 2015
2015
2015
2015
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/acceptedVersion
format article
status_str acceptedVersion
dc.identifier.none.fl_str_mv https://hdl.handle.net/2445/66853
url https://hdl.handle.net/2445/66853
dc.language.none.fl_str_mv Inglés
language_invalid_str_mv Inglés
dc.relation.none.fl_str_mv Versió postprint del document publicat a: http://dx.doi.org/10.1016/j.aca.2015.03.025
Analytica Chimica Acta, 2015, vol. 882, p. 1-21
http://dx.doi.org/10.1016/j.aca.2015.03.025
dc.rights.none.fl_str_mv cc-by-nc-nd (c) Elsevier B.V., 2015
http://creativecommons.org/licenses/by-nc-nd/3.0/es
info:eu-repo/semantics/openAccess
rights_invalid_str_mv cc-by-nc-nd (c) Elsevier B.V., 2015
http://creativecommons.org/licenses/by-nc-nd/3.0/es
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv 69 p.
application/pdf
dc.publisher.none.fl_str_mv Elsevier B.V.
publisher.none.fl_str_mv Elsevier B.V.
dc.source.none.fl_str_mv Articles publicats en revistes (Enginyeria Química i Química Analítica)
reponame:Recercat. Dipósit de la Recerca de Catalunya
instname:Varias* (Consorci de Biblioteques Universitáries de Catalunya, Centre de Serveis Científics i Acadèmics de Catalunya)
instname_str Varias* (Consorci de Biblioteques Universitáries de Catalunya, Centre de Serveis Científics i Acadèmics de Catalunya)
reponame_str Recercat. Dipósit de la Recerca de Catalunya
collection Recercat. Dipósit de la Recerca de Catalunya
repository.name.fl_str_mv
repository.mail.fl_str_mv
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score 15.198674

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