Surface modification of superduplex stainless steel with C and N: microstructural and nanomechanical insights

In this study, the effect of thermochemical processes, such as nitriding and carburizing, on the microstructural evolution of superdúplex stainless steel is presented. The objective is to find a correlation between the microstructure and the mechanical properties of the constitutive phases of this s...

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Detalhes bibliográficos
Autores: Biserova Tahchieva, Alisiya, Ortiz Membrado, Laia|||0000-0001-9646-3226, Benítez Iglesias, Raúl|||0000-0002-8782-9406, Rius Ayra, Josep Oriol, Llorca Isern, Núria|||0000-0003-0501-3866, Mateo García, Antonio Manuel|||0000-0001-8336-6128, Jiménez Piqué, Emilio|||0000-0002-6950-611X
Formato: artículo
Fecha de publicación:2024
País:España
Recursos:Universitat Politècnica de Catalunya (UPC)
Repositorio:UPCommons. Portal del coneixement obert de la UPC
Idioma:inglés
OAI Identifier:oai:upcommons.upc.edu:2117/428447
Acesso em linha:https://hdl.handle.net/2117/428447
https://dx.doi.org/10.1016/j.surfcoat.2024.131441
Access Level:acceso embargado
Palavra-chave:Superduplex stainless steel
Gas nitriding process
Carburizing
Nanoindentation
Micromechanical properties
Àrees temàtiques de la UPC::Enginyeria dels materials::Metal·lúrgia
Descrição
Resumo:In this study, the effect of thermochemical processes, such as nitriding and carburizing, on the microstructural evolution of superdúplex stainless steel is presented. The objective is to find a correlation between the microstructure and the mechanical properties of the constitutive phases of this stainless steel (i.e., austenite and ferrite) and analyze the diffusion elements influence on the precipitation of secondary phases, such as sigma (s), chi (¿), nitrides, and carbides. Hardness (H) and elastic modulus (E) maps were obtained by using a high-speed nanoindentation technique. H and E values for the individual phases were determined through the application of Gaussian Mixture Model statistical analysis. Assessments of the mechanical properties of the different phases were achieved by overlaying field emission-scanning electron microscopy micrographs. An excellent correlation between microstructure and small-scale mechanical properties was attained. Secondary phases have been detected and nanoindentation statistics have proven their influence on the mechanical properties.