Synthesis of Chiral Scaffolds Based on Polyfunctional Cyclobutane β-Amino Acids

Chiral scaffolds have been synthesized through selective transformations from conveniently protected cyclobutane β-amino acids. The obtained derivatives present additional functional groups, such as hydroxyl, carboxyl, or carbon-carbon triple bond, linked to the amino acid core through a flexible C...

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Detalles Bibliográficos
Autores: Verkh, Yaroslav|||0000-0003-0258-505X, Illa, Ona|||0000-0001-7390-4893, Ortuño Mingarro, Rosa María|||0000-0001-7635-7354
Tipo de recurso: artículo
Fecha de publicación:2021
País:España
Institución:Universitat Autònoma de Barcelona
Repositorio:Dipòsit Digital de Documents de la UAB
Idioma:inglés
OAI Identifier:oai:ddd.uab.cat:251394
Acceso en línea:https://ddd.uab.cat/record/251394
https://dx.doi.org/urn:doi:10.1002/ejoc.202101192
Access Level:acceso abierto
Palabra clave:Aminoacids
Chiral scaffolds
Peptidomimetics
Polyfuctional chemical platforms
Unnatural peptides
Descripción
Sumario:Chiral scaffolds have been synthesized through selective transformations from conveniently protected cyclobutane β-amino acids. The obtained derivatives present additional functional groups, such as hydroxyl, carboxyl, or carbon-carbon triple bond, linked to the amino acid core through a flexible C or C alkyl fragment. The resultant molecules are highly versatile to be used as chiral precursors for the production of polyfunctional chemical platforms. These can be suitable for the synthesis of complex molecules, through condensation reactions, such as peptide coupling, dehydration between a carboxylic acid and an alcohol, or click chemistry. To illustrate some of these possibilities, two hybrid tripeptides have been prepared as examples of their synthetic potential.