Synthesis of a new water-soluble highly Fe(III)-selective fluorescent chemosensor based on 4H-quinolizin-4-one

We describe the design, synthesis and studies of a new Fe(III)-selective fluorescent chemosensor in aqueous media based on a 4H-quinolizin-4-one (4b). This chemosensor exhibits high sensitivity and selectivity for the detection of Fe(III) in aqueous mixtures in the micromolar concentration range as...

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Detalles Bibliográficos
Autores: Gallardo-Rosas, David, Rosales-Vázquez, Luis D., Guevara Vela, José Manuel, Sandoval-Chávez, César I., Dorazco-González, Alejandro, Rocha-Rinza, Tomás, López-Cortés, José G., Ortega-Alfaro, M. Carmen
Tipo de recurso: artículo
Fecha de publicación:2025
País:España
Institución:Universidad Autónoma de Madrid
Repositorio:Biblos-e Archivo. Repositorio Institucional de la UAM
Idioma:inglés
OAI Identifier:oai:repositorio.uam.es:10486/718758
Acceso en línea:http://hdl.handle.net/10486/718758
https://dx.doi.org/10.1016/j.molstruc.2024.140753
Access Level:acceso abierto
Palabra clave:4H-quinolizin-4-one
Fe(III) detection
PET
fluorescence turn-off mechanism
fluorescent chemosensor
Química
Descripción
Sumario:We describe the design, synthesis and studies of a new Fe(III)-selective fluorescent chemosensor in aqueous media based on a 4H-quinolizin-4-one (4b). This chemosensor exhibits high sensitivity and selectivity for the detection of Fe(III) in aqueous mixtures in the micromolar concentration range as well as in the presence of other common interfering metal ions, making it a promising tool for the detection of Fe(III) with a limit of detection (LOD) of 13.15 μM in binary solvents DMSO/water, 1:1. Furthermore, this chemoreceptor exhibits a linear and stable fluorescent response over a range of 0 to 12 μM of Fe(III), with high affinity (3.13 × 106 M-2), which allows the quantitative determination of this metal ion. These results allow to envisage potential applications for the detection of Fe(III) in the diagnosis various of ferric-related diseases