Bismuthene - Tetrahedral DNA nanobioconjugate for virus detection

In this work, we present an electrochemical sensor for fast, low-cost, and easy detection of the SARS-CoV-2 spike protein in infected patients. The sensor is based on a selected combination of nanomaterials with a specific purpose. A bioconjugate formed by Few-layer bismuthene nanosheets (FLB) and t...

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Detalhes bibliográficos
Autores: Enebral-Romero, Estefanía, García-Fernández, Daniel, Gutiérrez-Gálvez, Laura, López-Diego, David, Luna, Mónica, García-Martín, Adrián, Salagre, Elena, Michel, Enrique G., Torres, Íñigo, Zamora, Félix, García-Mendiola, Tania, Lorenzo, Encarnación
Tipo de documento: artigo
Estado:Versão publicada
Data de publicação:2024
País:España
Recursos:Consejo Superior de Investigaciones Científicas (CSIC)
Repositório:DIGITAL.CSIC. Repositorio Institucional del CSIC
OAI Identifier:oai:digital.csic.es:10261/368554
Acesso em linha:http://hdl.handle.net/10261/368554
https://api.elsevier.com/content/abstract/scopus_id/85196157952
Access Level:Acceso aberto
Palavra-chave:Aptasensor
Bismuthene nanosheets
Nanostructured bioconjugate
SARS-CoV-2 aptamer-based tetrahedral DNA nanostructure (TDNapt)
Tetrahedral DNA nanostructure (TDN)
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dc.title.none.fl_str_mv Bismuthene - Tetrahedral DNA nanobioconjugate for virus detection
title Bismuthene - Tetrahedral DNA nanobioconjugate for virus detection
spellingShingle Bismuthene - Tetrahedral DNA nanobioconjugate for virus detection
Enebral-Romero, Estefanía
Aptasensor
Bismuthene nanosheets
Nanostructured bioconjugate
SARS-CoV-2 aptamer-based tetrahedral DNA nanostructure (TDNapt)
Tetrahedral DNA nanostructure (TDN)
title_short Bismuthene - Tetrahedral DNA nanobioconjugate for virus detection
title_full Bismuthene - Tetrahedral DNA nanobioconjugate for virus detection
title_fullStr Bismuthene - Tetrahedral DNA nanobioconjugate for virus detection
title_full_unstemmed Bismuthene - Tetrahedral DNA nanobioconjugate for virus detection
title_sort Bismuthene - Tetrahedral DNA nanobioconjugate for virus detection
dc.creator.none.fl_str_mv Enebral-Romero, Estefanía
García-Fernández, Daniel
Gutiérrez-Gálvez, Laura
López-Diego, David
Luna, Mónica
García-Martín, Adrián
Salagre, Elena
Michel, Enrique G.
Torres, Íñigo
Zamora, Félix
García-Mendiola, Tania
Lorenzo, Encarnación
author Enebral-Romero, Estefanía
author_facet Enebral-Romero, Estefanía
García-Fernández, Daniel
Gutiérrez-Gálvez, Laura
López-Diego, David
Luna, Mónica
García-Martín, Adrián
Salagre, Elena
Michel, Enrique G.
Torres, Íñigo
Zamora, Félix
García-Mendiola, Tania
Lorenzo, Encarnación
author_role author
author2 García-Fernández, Daniel
Gutiérrez-Gálvez, Laura
López-Diego, David
Luna, Mónica
García-Martín, Adrián
Salagre, Elena
Michel, Enrique G.
Torres, Íñigo
Zamora, Félix
García-Mendiola, Tania
Lorenzo, Encarnación
author2_role author
author
author
author
author
author
author
author
author
author
author
dc.contributor.none.fl_str_mv Agencia Estatal de Investigación (España)
Ministerio de Ciencia, Innovación y Universidades (España)
Ministerio de Ciencia e Innovación (España)
Comunidad de Madrid
European Commission
Consejo Superior de Investigaciones Científicas (España)
Ministerio de Economía y Competitividad (España)
Consejo Superior de Investigaciones Científicas [https://ror.org/02gfc7t72]
dc.subject.none.fl_str_mv Aptasensor
Bismuthene nanosheets
Nanostructured bioconjugate
SARS-CoV-2 aptamer-based tetrahedral DNA nanostructure (TDNapt)
Tetrahedral DNA nanostructure (TDN)
topic Aptasensor
Bismuthene nanosheets
Nanostructured bioconjugate
SARS-CoV-2 aptamer-based tetrahedral DNA nanostructure (TDNapt)
Tetrahedral DNA nanostructure (TDN)
description In this work, we present an electrochemical sensor for fast, low-cost, and easy detection of the SARS-CoV-2 spike protein in infected patients. The sensor is based on a selected combination of nanomaterials with a specific purpose. A bioconjugate formed by Few-layer bismuthene nanosheets (FLB) and tetrahedral DNA nanostructures (TDNs) is immobilized on Carbon Screen-Printed Electrodes (CSPE). The TDNs contain on the top vertex an aptamer that specifically binds to the SARS-CoV-2 spike protein, and a thiol group at the three basal vertices to anchor to the FLB. The TDNs are also marked with a redox indicator, Azure A (AA), which allows the direct detection of SARS-CoV-2 spike protein through changes in the current intensity of its electrolysis before and after the biorecognition reaction. The developed sensor can detect SARS-CoV-2 spike protein with a detection limit of 1.74 fg mL-1 directly in nasopharyngeal swab human samples. Therefore, this study offers a new strategy for rapid virus detection since it is versatile enough for different viruses and pathogens.
publishDate 2024
dc.date.none.fl_str_mv 2024
2024
2024
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https://api.elsevier.com/content/abstract/scopus_id/85196157952
url http://hdl.handle.net/10261/368554
https://api.elsevier.com/content/abstract/scopus_id/85196157952
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The underlying dataset has been published as supplementary material of the article in the publisher platform at https://doi.org/10.1016/j.bios.2024.116500
https://doi.org/10.1016/j.bios.2024.116500

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spelling Bismuthene - Tetrahedral DNA nanobioconjugate for virus detectionEnebral-Romero, EstefaníaGarcía-Fernández, DanielGutiérrez-Gálvez, LauraLópez-Diego, DavidLuna, MónicaGarcía-Martín, AdriánSalagre, ElenaMichel, Enrique G.Torres, ÍñigoZamora, FélixGarcía-Mendiola, TaniaLorenzo, EncarnaciónAptasensorBismuthene nanosheetsNanostructured bioconjugateSARS-CoV-2 aptamer-based tetrahedral DNA nanostructure (TDNapt)Tetrahedral DNA nanostructure (TDN)In this work, we present an electrochemical sensor for fast, low-cost, and easy detection of the SARS-CoV-2 spike protein in infected patients. The sensor is based on a selected combination of nanomaterials with a specific purpose. A bioconjugate formed by Few-layer bismuthene nanosheets (FLB) and tetrahedral DNA nanostructures (TDNs) is immobilized on Carbon Screen-Printed Electrodes (CSPE). The TDNs contain on the top vertex an aptamer that specifically binds to the SARS-CoV-2 spike protein, and a thiol group at the three basal vertices to anchor to the FLB. The TDNs are also marked with a redox indicator, Azure A (AA), which allows the direct detection of SARS-CoV-2 spike protein through changes in the current intensity of its electrolysis before and after the biorecognition reaction. The developed sensor can detect SARS-CoV-2 spike protein with a detection limit of 1.74 fg mL-1 directly in nasopharyngeal swab human samples. Therefore, this study offers a new strategy for rapid virus detection since it is versatile enough for different viruses and pathogens.This work has been financially supported by the Spanish Ministry of Economy and Competitiveness (PID2020-116728RB-I00, RED2022-134120-T), Spanish Ministry of Science, Innovation and Universities (TED2021-129738B–I00) and Community of Madrid (REACT-UE NANOCOV-CM, TRANSNANOAVANSENS, S2018/NMT-4349). Estefanía Enebral-Romero thanks the financial support of “Nanotecnología para detección del SARS-CoV-2 y sus variantes. NANOCOV” project and a contract as a predoctoral researcher funded by grant CEX2020-001039-S, supported by MCIN/AEI/10.13039/501100011033. Laura Gutiérrez-Gálvez was supported by a Formación del Profesorado Universitario (FPU) grant from the Spanish Ministry of Universities (FPU19/06309). Daniel García-Fernández and Adrián García-Martín were supported by a Programa Investigo grant from Autonomous Community of Madrid in the framework of the Plan de Recuperación, Transformación y Resiliencia financed by the European Union – NextGenerationEU (09-PIN1-00013.4/2022- 83rd and 66rd place, respectively). The authors acknowledge the support of the European Union (EU) and Horizon 2020 through Instruct Proposal PID: 21859, and the CRIOMECORR project (ESFRI-2019-01-CSIC-16) to the cryoEM CNB-CSIC facility. F. Z. acknowledges financial support from the Spanish Ministry of Science and Innovation, through the “María de Maeztu” Programme for Units of Excellence in R&D (CEX2023-001316-M, PDC2021-120782-C21, and PID2022-138908NB-C31), the “(MAD2D-CM)-UAM” project funded by Comunidad de Madrid, by the Recovery, Transformation and Resilience Plan, and by NextGenerationEU from the European Union. F.Z. also acknowledge support from the European Innovation Council under grant Agreement 101047081 (EVA). EGM acknowledges financial support from the Spanish Ministry of Science and Innovation, through the “María de Maeztu” Programme for Units of Excellence in R&D (CEX2018-000805-M) and through grant PID2021-123295NB-I00. We also acknowledge María U. González help with Fluorescence Microscopy and the service from the MiNa Laboratory at IMN, and funding from CM (project S2018/NMT-4291 TEC2SPACE), MINECO (project CSIC13-4E-1794) and EU (FEDER, FSE).Peer reviewedElsevierAgencia Estatal de Investigación (España)Ministerio de Ciencia, Innovación y Universidades (España)Ministerio de Ciencia e Innovación (España)Comunidad de MadridEuropean CommissionConsejo Superior de Investigaciones Científicas (España)Ministerio de Economía y Competitividad (España)Consejo Superior de Investigaciones Científicas [https://ror.org/02gfc7t72]202420242024info:eu-repo/semantics/articlehttp://purl.org/coar/resource_type/c_6501Publisher's versioninfo:eu-repo/semantics/publishedVersionapplication/pdfhttp://hdl.handle.net/10261/368554https://api.elsevier.com/content/abstract/scopus_id/85196157952reponame:DIGITAL.CSIC. 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