Integrated membrane process in organic media: combining organic solvent ultrafiltration, nanofiltration, and reverse osmosis to purify and concentrate the phenolic compounds from wet olive pomace.
[EN] Phenolic compounds from a hydroalcoholic extract of wet olive pomace were purified and concentrated by an integrated membrane process in organic media. First, UF010104 (Solsep BV) and UP005 (Microdyn Nadir) membranes were tested to be implemented in the ultrafiltration stage, with the aim of pu...
| Autores: | , , , |
|---|---|
| Tipo de recurso: | artículo |
| Fecha de publicación: | 2024 |
| País: | España |
| Institución: | Universitat Politècnica de València (UPV) |
| Repositorio: | RiuNet. Repositorio Institucional de la Universitat Politécnica de Valéncia |
| Idioma: | inglés |
| OAI Identifier: | oai:riunet.upv.es:10251/220390 |
| Acceso en línea: | https://riunet.upv.es/handle/10251/220390 |
| Access Level: | acceso abierto |
| Palabra clave: | Phenolic compounds Organic solvent ultrafiltration Organic solvent nanofiltration Reverse osmosis Integrated process Ethanol 06.- Garantizar la disponibilidad y la gestión sostenible del agua y el saneamiento para todos 09.- Desarrollar infraestructuras resilientes, promover la industrialización inclusiva y sostenible, y fomentar la innovación 12.- Garantizar las pautas de consumo y de producción sostenibles |
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oai:riunet.upv.es:10251/220390 |
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España |
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Integrated membrane process in organic media: combining organic solvent ultrafiltration, nanofiltration, and reverse osmosis to purify and concentrate the phenolic compounds from wet olive pomace.Sánchez-Arévalo, Carmen María|||0000-0001-6357-8107Vincent Vela, Maria Cinta|||0000-0001-8493-0165Alvarez Blanco, SilviaAldegheri, FaustoPhenolic compoundsOrganic solvent ultrafiltrationOrganic solvent nanofiltrationReverse osmosisIntegrated processEthanol06.- Garantizar la disponibilidad y la gestión sostenible del agua y el saneamiento para todos09.- Desarrollar infraestructuras resilientes, promover la industrialización inclusiva y sostenible, y fomentar la innovación12.- Garantizar las pautas de consumo y de producción sostenibles[EN] Phenolic compounds from a hydroalcoholic extract of wet olive pomace were purified and concentrated by an integrated membrane process in organic media. First, UF010104 (Solsep BV) and UP005 (Microdyn Nadir) membranes were tested to be implemented in the ultrafiltration stage, with the aim of purifying the extract and obtaining a permeate enriched in phenolic compounds. Despite the high flux observed with the UF010104 membrane (20.4 ± 0.7 L·h¿1·m¿2, at 2 bar), the UP005 membrane was selected because of a more suitable selectivity. Even though some secoiridoids were rejected, the permeate stream obtained with this embrane contained high concentrations of valuable simple phenols and phenolic acids, whereas sugars and macromolecules were retained. Then, the ultrafiltration permeate was ubjected to a nanofiltration step employing an NF270 membrane (DuPont) for a further purification and fractionation of the phenolic compounds. The permeate flux was 50.2 ± 0.2 L·h¿1·m¿2, working at 15 ar. Hydroxytyrosol and some phenolic acids (such as vanillic acid, caffeic acid, and ferulic acid) were recovered in the permeate, which was later concentrated by reverse osmosis employing an F90 membrane. The permeate flux obtained with this membrane was 15.3 ± 0.3 L·h¿1·m¿2. The concentrated phenolic mixture that was obtained may have important applications as a powerful ntioxidant and for the prevention of diabetes and neurodegenerative diseases.This research was funded by Generalitat Valencia, grant number CIAICO/2021/333. Additionally, a predoctoral grant PRE2018-08524 was funded by the Spanish Ministerio de Ciencia e Innovación (MCIN) /Agencia Estatal de Investigación (AEI)/10.13039/501100011033 and by European Social Fund (ESF) Investing in your future.MDPIInstituto Universitario de Seguridad Industrial, Radiofísica y MedioambientalDepartamento de Ingeniería Química y NuclearEscuela Técnica Superior de Ingeniería IndustrialGENERALITAT VALENCIANAAGENCIA ESTATAL DE INVESTIGACIONEuropean Regional Development FundRepositorio Institucional de la Universitat Politècnica de València Riunet20242024-05-01journal articlehttp://purl.org/coar/resource_type/c_6501VoRhttp://purl.org/coar/version/c_970fb48d4fbd8a85info:eu-repo/semantics/articleapplication/pdfhttps://riunet.upv.es/handle/10251/220390reponame:RiuNet. Repositorio Institucional de la Universitat Politécnica de Valénciainstname:Universitat Politècnica de València (UPV)InglésengAgencia Estatal de Investigación http://dx.doi.org/10.13039/501100011033 PRE2018-085245 AYUDA PARA CONTRATOS PREDOCTORALES PARA LA FORMACION DE DOCTORES-SANCHEZ AREVALO, CARMEN. PROYECTO: IMPLEMENTACION DE TECNOLOGIA DE MEMBRANAS PARA LA VALORIZACION DE LOS COMPUESTOS FENOLICOS PRESENTES EN LAS AGUAS RESIDUALESGeneralitat Valenciana https://doi.org/10.13039/501100003359 CIAICO%2F2021%2F333 RECUPERACION Y CONCENTRACION DE COMPUESTOS BIOACTIVOS DE ELEVADO VALOR A PARTIR DE RESIDUOS DE LA INDUSTRIA ALIMENTARIA MEDIANTEopen accesshttp://purl.org/coar/access_right/c_abf2Reconocimiento (by)http://creativecommons.org/licenses/by/4.0/info:eu-repo/semantics/openAccessoai:riunet.upv.es:10251/2203902026-06-13T07:49:27Z |
| dc.title.none.fl_str_mv |
Integrated membrane process in organic media: combining organic solvent ultrafiltration, nanofiltration, and reverse osmosis to purify and concentrate the phenolic compounds from wet olive pomace. |
| title |
Integrated membrane process in organic media: combining organic solvent ultrafiltration, nanofiltration, and reverse osmosis to purify and concentrate the phenolic compounds from wet olive pomace. |
| spellingShingle |
Integrated membrane process in organic media: combining organic solvent ultrafiltration, nanofiltration, and reverse osmosis to purify and concentrate the phenolic compounds from wet olive pomace. Sánchez-Arévalo, Carmen María|||0000-0001-6357-8107 Phenolic compounds Organic solvent ultrafiltration Organic solvent nanofiltration Reverse osmosis Integrated process Ethanol 06.- Garantizar la disponibilidad y la gestión sostenible del agua y el saneamiento para todos 09.- Desarrollar infraestructuras resilientes, promover la industrialización inclusiva y sostenible, y fomentar la innovación 12.- Garantizar las pautas de consumo y de producción sostenibles |
| title_short |
Integrated membrane process in organic media: combining organic solvent ultrafiltration, nanofiltration, and reverse osmosis to purify and concentrate the phenolic compounds from wet olive pomace. |
| title_full |
Integrated membrane process in organic media: combining organic solvent ultrafiltration, nanofiltration, and reverse osmosis to purify and concentrate the phenolic compounds from wet olive pomace. |
| title_fullStr |
Integrated membrane process in organic media: combining organic solvent ultrafiltration, nanofiltration, and reverse osmosis to purify and concentrate the phenolic compounds from wet olive pomace. |
| title_full_unstemmed |
Integrated membrane process in organic media: combining organic solvent ultrafiltration, nanofiltration, and reverse osmosis to purify and concentrate the phenolic compounds from wet olive pomace. |
| title_sort |
Integrated membrane process in organic media: combining organic solvent ultrafiltration, nanofiltration, and reverse osmosis to purify and concentrate the phenolic compounds from wet olive pomace. |
| dc.creator.none.fl_str_mv |
Sánchez-Arévalo, Carmen María|||0000-0001-6357-8107 Vincent Vela, Maria Cinta|||0000-0001-8493-0165 Alvarez Blanco, Silvia Aldegheri, Fausto |
| author |
Sánchez-Arévalo, Carmen María|||0000-0001-6357-8107 |
| author_facet |
Sánchez-Arévalo, Carmen María|||0000-0001-6357-8107 Vincent Vela, Maria Cinta|||0000-0001-8493-0165 Alvarez Blanco, Silvia Aldegheri, Fausto |
| author_role |
author |
| author2 |
Vincent Vela, Maria Cinta|||0000-0001-8493-0165 Alvarez Blanco, Silvia Aldegheri, Fausto |
| author2_role |
author author author |
| dc.contributor.none.fl_str_mv |
Instituto Universitario de Seguridad Industrial, Radiofísica y Medioambiental Departamento de Ingeniería Química y Nuclear Escuela Técnica Superior de Ingeniería Industrial GENERALITAT VALENCIANA AGENCIA ESTATAL DE INVESTIGACION European Regional Development Fund Repositorio Institucional de la Universitat Politècnica de València Riunet |
| dc.subject.none.fl_str_mv |
Phenolic compounds Organic solvent ultrafiltration Organic solvent nanofiltration Reverse osmosis Integrated process Ethanol 06.- Garantizar la disponibilidad y la gestión sostenible del agua y el saneamiento para todos 09.- Desarrollar infraestructuras resilientes, promover la industrialización inclusiva y sostenible, y fomentar la innovación 12.- Garantizar las pautas de consumo y de producción sostenibles |
| topic |
Phenolic compounds Organic solvent ultrafiltration Organic solvent nanofiltration Reverse osmosis Integrated process Ethanol 06.- Garantizar la disponibilidad y la gestión sostenible del agua y el saneamiento para todos 09.- Desarrollar infraestructuras resilientes, promover la industrialización inclusiva y sostenible, y fomentar la innovación 12.- Garantizar las pautas de consumo y de producción sostenibles |
| description |
[EN] Phenolic compounds from a hydroalcoholic extract of wet olive pomace were purified and concentrated by an integrated membrane process in organic media. First, UF010104 (Solsep BV) and UP005 (Microdyn Nadir) membranes were tested to be implemented in the ultrafiltration stage, with the aim of purifying the extract and obtaining a permeate enriched in phenolic compounds. Despite the high flux observed with the UF010104 membrane (20.4 ± 0.7 L·h¿1·m¿2, at 2 bar), the UP005 membrane was selected because of a more suitable selectivity. Even though some secoiridoids were rejected, the permeate stream obtained with this embrane contained high concentrations of valuable simple phenols and phenolic acids, whereas sugars and macromolecules were retained. Then, the ultrafiltration permeate was ubjected to a nanofiltration step employing an NF270 membrane (DuPont) for a further purification and fractionation of the phenolic compounds. The permeate flux was 50.2 ± 0.2 L·h¿1·m¿2, working at 15 ar. Hydroxytyrosol and some phenolic acids (such as vanillic acid, caffeic acid, and ferulic acid) were recovered in the permeate, which was later concentrated by reverse osmosis employing an F90 membrane. The permeate flux obtained with this membrane was 15.3 ± 0.3 L·h¿1·m¿2. The concentrated phenolic mixture that was obtained may have important applications as a powerful ntioxidant and for the prevention of diabetes and neurodegenerative diseases. |
| publishDate |
2024 |
| dc.date.none.fl_str_mv |
2024 2024-05-01 |
| dc.type.none.fl_str_mv |
journal article http://purl.org/coar/resource_type/c_6501 VoR http://purl.org/coar/version/c_970fb48d4fbd8a85 |
| dc.type.openaire.fl_str_mv |
info:eu-repo/semantics/article |
| format |
article |
| dc.identifier.none.fl_str_mv |
https://riunet.upv.es/handle/10251/220390 |
| url |
https://riunet.upv.es/handle/10251/220390 |
| dc.language.none.fl_str_mv |
Inglés eng |
| language_invalid_str_mv |
Inglés |
| language |
eng |
| dc.relation.none.fl_str_mv |
Agencia Estatal de Investigación http://dx.doi.org/10.13039/501100011033 PRE2018-085245 AYUDA PARA CONTRATOS PREDOCTORALES PARA LA FORMACION DE DOCTORES-SANCHEZ AREVALO, CARMEN. PROYECTO: IMPLEMENTACION DE TECNOLOGIA DE MEMBRANAS PARA LA VALORIZACION DE LOS COMPUESTOS FENOLICOS PRESENTES EN LAS AGUAS RESIDUALES Generalitat Valenciana https://doi.org/10.13039/501100003359 CIAICO%2F2021%2F333 RECUPERACION Y CONCENTRACION DE COMPUESTOS BIOACTIVOS DE ELEVADO VALOR A PARTIR DE RESIDUOS DE LA INDUSTRIA ALIMENTARIA MEDIANTE |
| dc.rights.none.fl_str_mv |
open access http://purl.org/coar/access_right/c_abf2 Reconocimiento (by) http://creativecommons.org/licenses/by/4.0/ |
| dc.rights.openaire.fl_str_mv |
info:eu-repo/semantics/openAccess |
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open access http://purl.org/coar/access_right/c_abf2 Reconocimiento (by) http://creativecommons.org/licenses/by/4.0/ |
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openAccess |
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application/pdf |
| dc.publisher.none.fl_str_mv |
MDPI |
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MDPI |
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reponame:RiuNet. Repositorio Institucional de la Universitat Politécnica de Valéncia instname:Universitat Politècnica de València (UPV) |
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Universitat Politècnica de València (UPV) |
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RiuNet. Repositorio Institucional de la Universitat Politécnica de Valéncia |
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RiuNet. Repositorio Institucional de la Universitat Politécnica de Valéncia |
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15.811543 |