Chiral micellar electrokinetic chromatography

The potential of Micellar Electrokinetic Chromatography to achieve enantiomeric separations is reviewed in this article. The separation principles and the most frequently employed separation strategies to achieve chiral separations by Micellar Electrokinetic Chromatography are described. The use of...

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Detalles Bibliográficos
Autores: Marina Alegre, María Luisa|||0000-0002-5583-1624, Castro Puyana, María|||0000-0003-1412-4103, Salido Fortuna, Sandra|||0000-0002-0792-3559
Tipo de recurso: artículo
Fecha de publicación:2020
País:España
Institución:Universidad de Alcalá (UAH)
Repositorio:e_Buah Biblioteca Digital Universidad de Alcalá
Idioma:inglés
OAI Identifier:oai:ebuah.uah.es:10017/47097
Acceso en línea:http://hdl.handle.net/10017/47097
https://dx.doi.org/10.1016/j.chroma.2020.461383
Access Level:acceso abierto
Palabra clave:Enantiomeric separations
Micellar Electrokinetic Chromatography
Fundamentals
Chiral separation strategies
analytical applications
Química
Chemistry
Descripción
Sumario:The potential of Micellar Electrokinetic Chromatography to achieve enantiomeric separations is reviewed in this article. The separation principles and the most frequently employed separation strategies to achieve chiral separations by Micellar Electrokinetic Chromatography are described. The use of chiral micellar systems alone or combined with other micellar systems or chiral selectors, as well as of mixtures of achiral micellar systems with chiral selectors is discussed together with the effect of different additives present in the separation medium. Indirect methods based on the derivatization of analytes with chiral derivatizing reagents and the use of achiral micelles are also considered. Preconcentration techniques employed to improve sensitivity and the main approaches developed to facilitate the coupling with Mass Spectrometry are included. The most recent and relevant methodologies developed by chiral Micellar Electrokinetic Chromatography and their applications in different fields are presented.