10β-Hydroxy-1,4-estradiene-3,17-dione

C18H22=3 Mr=286.4, orthorhombic, P212121, a=7.014(2), b=12.176(4), c=17.648(4)A, V=1507.2 A3, Z=4, Dx=1.26 Mg m-3m (Mo Ka)=0.71069 A, µ=0.079 mm-1m F(000)=616, T ca 130 K, R=0.109 for all 2506 unique reflections within -1sinO=0.70 A-1; the absolute configuration was not determined. The relative ster...

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Detalles Bibliográficos
Autores: Bieri, J. H., Prewo, R., Briansó, José Luis, Piniella, J. Francesc
Tipo de recurso: artículo
Fecha de publicación:1985
País:España
Institución:Universitat Autònoma de Barcelona
Repositorio:Dipòsit Digital de Documents de la UAB
Idioma:inglés
OAI Identifier:oai:ddd.uab.cat:27757
Acceso en línea:https://ddd.uab.cat/record/27757
https://dx.doi.org/urn:doi:10.1107/S0108270185008435
Access Level:acceso abierto
Palabra clave:Cristal·lografia
Crystallography
Descripción
Sumario:C18H22=3 Mr=286.4, orthorhombic, P212121, a=7.014(2), b=12.176(4), c=17.648(4)A, V=1507.2 A3, Z=4, Dx=1.26 Mg m-3m (Mo Ka)=0.71069 A, µ=0.079 mm-1m F(000)=616, T ca 130 K, R=0.109 for all 2506 unique reflections within -1sinO=0.70 A-1; the absolute configuration was not determined. The relative stereochemistry at C(10) is established. The unsaturated ring is essentially planar; the two central rings are in the chair conformation and the five-membered ring adopts the envelope conformation.