Iron-Catalyzed Radical Intermolecular Addition of Unbiased Alkenes to Aldehydes

The intermolecular reductive radical coupling of aldehydes with nonactivated alkenes, employing metal hydride atom transfer (MHAT) catalysis with a combination of FeII and FeIII salts, is described. This constitutes the first use of aldehydes as viable acceptor groups in MHAT reactions. The insights...

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Detalles Bibliográficos
Autores: Saladrigas, Mar, Puig Bosch, Jordi, Bonjoch i Sesé, Josep, Bradshaw, Ben
Tipo de recurso: artículo
Estado:Versión aceptada para publicación
Fecha de publicación:2020
País:España
Institución:Universidad de Barcelona
Repositorio:Dipòsit Digital de la UB
OAI Identifier:oai:diposit.ub.edu:2445/173441
Acceso en línea:https://hdl.handle.net/2445/173441
Access Level:acceso abierto
Palabra clave:Alquens
Catàlisi
Enllaços químics
Química orgànica
Alkenes
Catalysis
Chemical bonds
Organic chemistry
Descripción
Sumario:The intermolecular reductive radical coupling of aldehydes with nonactivated alkenes, employing metal hydride atom transfer (MHAT) catalysis with a combination of FeII and FeIII salts, is described. This constitutes the first use of aldehydes as viable acceptor groups in MHAT reactions. The insights gained in this study led to the reexamination of the previously reported intramolecular version of the reaction, and the addition of FeII salts allowed the development of a more efficient second-generation approach.