A review of sample preparation and its influence on pH determination in concrete samples

If we are to monitor the chemical processes in cementitious materials, then pH assays in the pore solutions of cement pastes, mortars, and concretes are of key importance. However, there is no standard method that regulates the sample-preparation method for pH determination. The state-of-the-art of...

ver descrição completa

Detalhes bibliográficos
Autores: Manso Blanco, Sandra|||0000-0002-2712-5976, Aguado de Cea, Antonio|||0000-0001-5542-6365
Tipo de documento: artigo
Data de publicação:2017
País:España
Recursos:Universitat Politècnica de Catalunya (UPC)
Repositório:UPCommons. Portal del coneixement obert de la UPC
Idioma:inglês
OAI Identifier:oai:upcommons.upc.edu:2117/102144
Acesso em linha:https://hdl.handle.net/2117/102144
https://dx.doi.org/10.3989/mc.2017.08515
Access Level:Acceso aberto
Palavra-chave:Cement composites--Analysis
pH
Concrete
Mortar
Cement paste
Pore solution
Ciment -- Química
Àrees temàtiques de la UPC::Enginyeria civil::Materials i estructures::Materials i estructures de formigó
Descrição
Resumo:If we are to monitor the chemical processes in cementitious materials, then pH assays in the pore solutions of cement pastes, mortars, and concretes are of key importance. However, there is no standard method that regulates the sample-preparation method for pH determination. The state-of-the-art of different methods for pH determination in cementitious materials is presented in this paper and the influence of sample preparation in each case. Moreover, an experimental campaign compares three different techniques for pH determination. Its results contribute to establishing a basic criterion to help researchers select the most suitable method, depending on the purpose of the research. A simple tool is described for selecting the easiest and the most economic pH determination method, depending on the objective; especially for researchers and those with limited experience in this field.