Validation of an Inductively Coupled Plasma-Optical Emission Spectrometry Method for the Determination of Major Elements in Farmed Rainbow Trout (Oncorhynchus mykiss)

An inductively coupled plasma−optical emission spectrometry method was optimized and validated for the determination of major elements (Ca, K, Mg, Na and P) in cultivated freshwater fish (rainbow trout Oncorhynchus mykiss). The method was validated by analysis of a Certified Reference Material, cons...

Descripción completa

Detalles Bibliográficos
Autores: Velasco Villar, Susana, Ortiz Vera, Luis Tomás, Rodríguez, M. L., Rebolé Garrido, Almudena, Treviño, J., Benito, T., López De Andrés, María Sol, Gómez-Pinilla, María Isabel
Tipo de recurso: artículo
Fecha de publicación:2017
País:España
Institución:Universidad Complutense de Madrid (UCM)
Repositorio:Docta Complutense
Idioma:inglés
OAI Identifier:oai:docta.ucm.es:20.500.14352/18597
Acceso en línea:https://hdl.handle.net/20.500.14352/18597
Access Level:acceso abierto
Palabra clave:548:53
Inductively coupled plasma-optical emission spectrometry
Microwave digestion
Major element determination
Method and validation
Fish
Rainbow trout
Food composition
Oncorhynchus mykiss
Cristalografía (Geología)
id ES_c8a0481c44bf5bb10a09453d0ba9bc2a
oai_identifier_str oai:docta.ucm.es:20.500.14352/18597
network_acronym_str ES
network_name_str España
repository_id_str
spelling Validation of an Inductively Coupled Plasma-Optical Emission Spectrometry Method for the Determination of Major Elements in Farmed Rainbow Trout (Oncorhynchus mykiss)Velasco Villar, SusanaOrtiz Vera, Luis TomásRodríguez, M. L.Rebolé Garrido, AlmudenaTreviño, J.Benito, T.López De Andrés, María SolGómez-Pinilla, María Isabel548:53Inductively coupled plasma-optical emission spectrometryMicrowave digestionMajor element determinationMethod and validationFishRainbow troutFood compositionOncorhynchus mykissCristalografía (Geología)An inductively coupled plasma−optical emission spectrometry method was optimized and validated for the determination of major elements (Ca, K, Mg, Na and P) in cultivated freshwater fish (rainbow trout Oncorhynchus mykiss). The method was validated by analysis of a Certified Reference Material, consisting in a frozen tissue homogenate from lake trout (Salvelinus namaycush namaycush). The linearity of this method was very good, as evidenced by the coefficients of correlation (r) for calibration graphs that were higher than 0.9999 in all cases and by linearity test (response factor <5% and relative calibration graph slope <2%). Accuracy, expressed as relative recovery (%) in comparison with certified concentration ranged from 100 to 109%, and precision, expressed as residual standard deviation (%) ranged from 1.2 to 6.5% (repeatability) and from 1.0 to 9.6% (reproducibility). The limit of quantification ranged from 4 ng/mL (Ca and Mg) to 203 ng/mL (P). The optimized method was applied to major element determination in skin and muscle samples from rainbow trout fillets.Nauka/Interperiodica. Editor comerical Springer VerlagUniversidad Complutense de Madrid20172017-09-0120172017-09-01journal articlehttp://purl.org/coar/resource_type/c_6501info:eu-repo/semantics/articleapplication/pdfhttps://hdl.handle.net/20.500.14352/18597reponame:Docta Complutenseinstname:Universidad Complutense de Madrid (UCM)Inglésengopen accesshttp://purl.org/coar/access_right/c_abf2info:eu-repo/semantics/openAccessoai:docta.ucm.es:20.500.14352/185972026-06-02T12:44:21Z
dc.title.none.fl_str_mv Validation of an Inductively Coupled Plasma-Optical Emission Spectrometry Method for the Determination of Major Elements in Farmed Rainbow Trout (Oncorhynchus mykiss)
title Validation of an Inductively Coupled Plasma-Optical Emission Spectrometry Method for the Determination of Major Elements in Farmed Rainbow Trout (Oncorhynchus mykiss)
spellingShingle Validation of an Inductively Coupled Plasma-Optical Emission Spectrometry Method for the Determination of Major Elements in Farmed Rainbow Trout (Oncorhynchus mykiss)
Velasco Villar, Susana
548:53
Inductively coupled plasma-optical emission spectrometry
Microwave digestion
Major element determination
Method and validation
Fish
Rainbow trout
Food composition
Oncorhynchus mykiss
Cristalografía (Geología)
title_short Validation of an Inductively Coupled Plasma-Optical Emission Spectrometry Method for the Determination of Major Elements in Farmed Rainbow Trout (Oncorhynchus mykiss)
title_full Validation of an Inductively Coupled Plasma-Optical Emission Spectrometry Method for the Determination of Major Elements in Farmed Rainbow Trout (Oncorhynchus mykiss)
title_fullStr Validation of an Inductively Coupled Plasma-Optical Emission Spectrometry Method for the Determination of Major Elements in Farmed Rainbow Trout (Oncorhynchus mykiss)
title_full_unstemmed Validation of an Inductively Coupled Plasma-Optical Emission Spectrometry Method for the Determination of Major Elements in Farmed Rainbow Trout (Oncorhynchus mykiss)
title_sort Validation of an Inductively Coupled Plasma-Optical Emission Spectrometry Method for the Determination of Major Elements in Farmed Rainbow Trout (Oncorhynchus mykiss)
dc.creator.none.fl_str_mv Velasco Villar, Susana
Ortiz Vera, Luis Tomás
Rodríguez, M. L.
Rebolé Garrido, Almudena
Treviño, J.
Benito, T.
López De Andrés, María Sol
Gómez-Pinilla, María Isabel
author Velasco Villar, Susana
author_facet Velasco Villar, Susana
Ortiz Vera, Luis Tomás
Rodríguez, M. L.
Rebolé Garrido, Almudena
Treviño, J.
Benito, T.
López De Andrés, María Sol
Gómez-Pinilla, María Isabel
author_role author
author2 Ortiz Vera, Luis Tomás
Rodríguez, M. L.
Rebolé Garrido, Almudena
Treviño, J.
Benito, T.
López De Andrés, María Sol
Gómez-Pinilla, María Isabel
author2_role author
author
author
author
author
author
author
dc.contributor.none.fl_str_mv Universidad Complutense de Madrid
dc.subject.none.fl_str_mv 548:53
Inductively coupled plasma-optical emission spectrometry
Microwave digestion
Major element determination
Method and validation
Fish
Rainbow trout
Food composition
Oncorhynchus mykiss
Cristalografía (Geología)
topic 548:53
Inductively coupled plasma-optical emission spectrometry
Microwave digestion
Major element determination
Method and validation
Fish
Rainbow trout
Food composition
Oncorhynchus mykiss
Cristalografía (Geología)
description An inductively coupled plasma−optical emission spectrometry method was optimized and validated for the determination of major elements (Ca, K, Mg, Na and P) in cultivated freshwater fish (rainbow trout Oncorhynchus mykiss). The method was validated by analysis of a Certified Reference Material, consisting in a frozen tissue homogenate from lake trout (Salvelinus namaycush namaycush). The linearity of this method was very good, as evidenced by the coefficients of correlation (r) for calibration graphs that were higher than 0.9999 in all cases and by linearity test (response factor <5% and relative calibration graph slope <2%). Accuracy, expressed as relative recovery (%) in comparison with certified concentration ranged from 100 to 109%, and precision, expressed as residual standard deviation (%) ranged from 1.2 to 6.5% (repeatability) and from 1.0 to 9.6% (reproducibility). The limit of quantification ranged from 4 ng/mL (Ca and Mg) to 203 ng/mL (P). The optimized method was applied to major element determination in skin and muscle samples from rainbow trout fillets.
publishDate 2017
dc.date.none.fl_str_mv 2017
2017-09-01
2017
2017-09-01
dc.type.none.fl_str_mv journal article
http://purl.org/coar/resource_type/c_6501
dc.type.openaire.fl_str_mv info:eu-repo/semantics/article
format article
dc.identifier.none.fl_str_mv https://hdl.handle.net/20.500.14352/18597
url https://hdl.handle.net/20.500.14352/18597
dc.language.none.fl_str_mv Inglés
eng
language_invalid_str_mv Inglés
language eng
dc.rights.none.fl_str_mv open access
http://purl.org/coar/access_right/c_abf2
dc.rights.openaire.fl_str_mv info:eu-repo/semantics/openAccess
rights_invalid_str_mv open access
http://purl.org/coar/access_right/c_abf2
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
dc.publisher.none.fl_str_mv Nauka/Interperiodica. Editor comerical Springer Verlag
publisher.none.fl_str_mv Nauka/Interperiodica. Editor comerical Springer Verlag
dc.source.none.fl_str_mv reponame:Docta Complutense
instname:Universidad Complutense de Madrid (UCM)
instname_str Universidad Complutense de Madrid (UCM)
reponame_str Docta Complutense
collection Docta Complutense
repository.name.fl_str_mv
repository.mail.fl_str_mv
_version_ 1869419301991088128
score 15,301603

Similares en LA Referencia