Effect of the sulphonating agent on the catalytic behavior of activated carbons in the dehydration reaction of fructose in DMSO

A series of -SO3R functionalized activated carbons (R=H, O, aryl) were prepared and applied in fructose dehydration reaction to 5-hydroxymethylfurfural. Different sulphonating methods introduce groups on catalyst surface with distinct donor-acceptor and hydrophilic properties. Their nature influence...

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Detalles Bibliográficos
Autores: Bounoukta, Charf Eddine, Megías Sayago, Cristina, Ivanova, Svetlana, Penkova, Anna Dimitrova, Ammari, Fatima, Centeno Gallego, Miguel Ángel, Odriozola Gordón, José Antonio
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2021
País:España
Institución:Universidad de Sevilla (US)
Repositorio:idUS. Depósito de Investigación de la Universidad de Sevilla
OAI Identifier:oai:idus.us.es:11441/166196
Acceso en línea:https://hdl.handle.net/11441/166196
https://doi.org/10.1016/j.apcata.2021.118108
Access Level:acceso abierto
Palabra clave:Activated carbon
Fructose dehydration
HMF production
Sulphonating agent
Descripción
Sumario:A series of -SO3R functionalized activated carbons (R=H, O, aryl) were prepared and applied in fructose dehydration reaction to 5-hydroxymethylfurfural. Different sulphonating methods introduce groups on catalyst surface with distinct donor-acceptor and hydrophilic properties. Their nature influences significantly not only activated carbon's textural and chemical properties but also the product yields and selectivity in fructose dehydration reaction. The viability of the solvent free reaction was also investigated and compared to the performance of the catalyst series in presence of DMSO, where the best catalytic results were obtained.