Biocarbonates Derived from CO2 and Terpenes: Molecular Design for Aqueous Mixture Treatment Driven by COSMO-RS

In this work, the use of plant-derived raw materials, such as terpenes, gives great strength from a sustainability perspective and enables dealing with the biocarbonate concept. Biocarbonates are produced only from CO2and residues or bio-derived compounds, describing cycloaddition reactions that cou...

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Detalhes bibliográficos
Autores: Belinchón Abenójar, Alejandro, Hernández Muñoz, Elisa, Vázquez, Javier, Santiago Lorenzo, Rubén, Moya Álamo, Cristian, Larriba, Marcos, Navarro Tejedor, Pablo, Palomar Herrero, José Francisco
Formato: artículo
Fecha de publicación:2022
País:España
Recursos:Universidad Autónoma de Madrid
Repositorio:Biblos-e Archivo. Repositorio Institucional de la UAM
Idioma:inglés
OAI Identifier:oai:repositorio.uam.es:10486/704335
Acesso em linha:http://hdl.handle.net/10486/704335
https://dx.doi.org/10.1021/acssuschemeng.2c02993
Access Level:acceso abierto
Palavra-chave:Biocarbonate
CO conversion 2
COSMO-RS
Liquid-liquid extraction
Terpene
Química
Descrição
Resumo:In this work, the use of plant-derived raw materials, such as terpenes, gives great strength from a sustainability perspective and enables dealing with the biocarbonate concept. Biocarbonates are produced only from CO2and residues or bio-derived compounds, describing cycloaddition reactions that couple CO2and a terpene, the latter after epoxidation, avoiding environmental charges from petroleum-derived epoxides. In this work, a comprehensive database (derived from 30 terpenes) accounting bioepoxides and corresponding biocarbonates was developed, by means of molecular simulation. Optimized structures realized by the DFT method allow using a priori tools to scan the possible applications of this new class of sustainable solvents. Using a COnductor-like Screening Model for Realistic Solvents, different biocarbonates were evaluated for their physical properties and capacity to remove value-Added or contaminant solutes from aqueous mixtures, namely, furfural, phenolic compounds, and volatile fatty acids. It was found that biocarbonates derived from terpenes generally present a higher affinity for solutes in comparison with neat terpenes. Indeed, biocarbonates allowed achieving the recovery of 99% of phenol, 98% of furfural, and 87% of acetic acid, also pointing to an advantageous scenario of higher boiling points and densities and comparable solvent losses in the aqueous phase to terpenes