AMPHIBIAN CSIC experimental data insitu exsitu PXRD NPD [Dataset]
The different datasets are divided in folders as follows: 1. In situ experiments. The article is based on 7 different in situ experiments: a. 400C_5mLmin_fr10; b. 400C_10mLmin_fr23; c. 400C_20mLmin_fr6; d. 400C_30mLmin_fr12; e. 300C_10mLmin_fr4; f. 350C_10mLmin_fr18; g. 500C_10mLmin_fr9. (Due to spa...
| Autores: | , , , , , , , , |
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| Tipo de recurso: | conjunto de datos |
| Fecha de publicación: | 2019 |
| País: | España |
| Institución: | Consejo Superior de Investigaciones Científicas (CSIC) |
| Repositorio: | DIGITAL.CSIC. Repositorio Institucional del CSIC |
| OAI Identifier: | oai:digital.csic.es:10261/174043 |
| Acceso en línea: | http://hdl.handle.net/10261/174043 |
| Access Level: | acceso abierto |
| Palabra clave: | Spinel ferrites CoFe2O4 Cobalt ferrite CoFe Nanocrystallites Magnetic nanoparticles Exchange-coupling Composites In-situ Ex-situ Rietveld refinements Powder x-ray diffraction PXRD Neutron powder diffraction NPD Elemental composition Vibrating sample magnetometry VSM Permanent magnets |
| Sumario: | The different datasets are divided in folders as follows: 1. In situ experiments. The article is based on 7 different in situ experiments: a. 400C_5mLmin_fr10; b. 400C_10mLmin_fr23; c. 400C_20mLmin_fr6; d. 400C_30mLmin_fr12; e. 300C_10mLmin_fr4; f. 350C_10mLmin_fr18; g. 500C_10mLmin_fr9. (Due to space limitations, only the data corresponding to the experiment c were uploaded to this repository. The remaining data are accessible through private communication with Cecilia Granados-Miralles, c.granados.miralles@icv.csic.es). The folder “c_400C_20mLmin_fr6” contains in situ PXRD data (time resolution=5 s) collected during reduction at the temperature and gas flow indicated in the folder name (i.e. 400C_20mLmin stands for 400 °C and 20 mL/min). The temperature indicated in the file names is the set temperature but the sample temperature is the indicated in the folder name (i.e. Tset430 led to a sample temperature of 400 °C). Heating started on the frame indicated in the folder name (i.e. fr6 stands for frame 6). This folder contains 2D-diffraction images in *.tif format, which may be opened with the Python-based program for on-the-fly data processing and exploration of two-dimensional X-ray diffraction area detector data, available for free download at http://www.clemensprescher.com/programs/dioptas. |
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