The effect of support surface hydroxyls on selective CO methanation with Ru based catalysts

The aim of this work was to clarify the effect of the support on CO selective methanation with Ru/TiO2 catalysts. TPR, XRD and TEM measurements confirmed that the changes in the activity and selectivity should be ascribed to anatase:rutile ratio, RuO2 +TiO2 solid solution formation, as well as the m...

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Detalles Bibliográficos
Autores: Martínez Tejada, Leidy Marcela, Muñoz Bernabé, Antonio, Pérez Flores, Alejandro, Laguna Espitia, Óscar Hernando, Bobadilla Baladrón, Luis Francisco, Centeno, Miguel Ángel, Odriozola Gordón, José Antonio
Tipo de recurso: artículo
Estado:Versión aceptada para publicación
Fecha de publicación:2022
País:España
Institución:Universidad de Sevilla (US)
Repositorio:idUS. Depósito de Investigación de la Universidad de Sevilla
OAI Identifier:oai:idus.us.es:11441/179053
Acceso en línea:https://hdl.handle.net/11441/179053
https://doi.org/10.1016/j.apcata.2022.118678
Access Level:acceso abierto
Palabra clave:Ru/TiO2 catalysts
TiO2 rutile
TiO2 anatase
RuO2 rutile
CO methanation
CO2 methanation
Support surface hydroxyls
Descripción
Sumario:The aim of this work was to clarify the effect of the support on CO selective methanation with Ru/TiO2 catalysts. TPR, XRD and TEM measurements confirmed that the changes in the activity and selectivity should be ascribed to anatase:rutile ratio, RuO2 +TiO2 solid solution formation, as well as the metal content and the thermal treatment used. All these characteristics result in active and selective catalysts in which the suppression of the reverse water gas shift reaction was observed. The catalytic performance must be explained by both the formation of more active Ru species as a result of support influence and the higher Ru dispersion. The study allows to conclude that for CO activation the role of support surface hydroxyls seems to be determinant for both the activity and selectivity of Ru/TiO2 catalysts.