A Fluorescent Cage for Supramolecular Sensing of 3-Nitrotyrosine in Human Blood Serum

3-Nitrotyrosine (NT) is generated by the action of peroxynitrite and other reactive nitrogen species (RNS), and as a consequence it is accumulated in inflammation-associated conditions. This is particularly relevant in kidney disease, where NT concentration in blood is considerably high. Therefore,...

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Detalles Bibliográficos
Autores: Pérez Márquez, Lidia A., Perretti, Marcelle D., García Rodríguez, Raúl, Lahoz, Fernando, Carrillo, Romen
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2022
País:España
Institución:Universidad de Valladolid
Repositorio:UVaDOC. Repositorio Documental de la Universidad de Valladolid
OAI Identifier:oai:uvadoc.uva.es:10324/65522
Acceso en línea:https://doi.org/10.1002/anie.202205403
https://uvadoc.uva.es/handle/10324/65522
Access Level:acceso abierto
Palabra clave:Química inorgánica
Molecular Cages
lecular Recognition
Nitrotyrosine
Sensors Tetraphenylethene
2301.06 Fluorimetría
2301 Química Analítica
Descripción
Sumario:3-Nitrotyrosine (NT) is generated by the action of peroxynitrite and other reactive nitrogen species (RNS), and as a consequence it is accumulated in inflammation-associated conditions. This is particularly relevant in kidney disease, where NT concentration in blood is considerably high. Therefore, NT is a crucial biomarker of renal damage, although it has been underestimated in clinical diagnosis due to the lack of an appropriate sensing method. Herein we report the first fluorescent supramolecular sensor for such a relevant compound: Fluorescence by rotational restriction of tetraphenylethenes (TPE) in a covalent cage is selectively quenched in human blood serum by 3-nitrotyrosine (NT) that binds to the cage with high affinity, allowing a limit of detection within the reported physiological concentrations of NT in chronic kidney disease.