BiVO4-Based Photocatalysts for the Degradation of Antibiotics in Wastewater: Calcination Role after Solvothermal Synthesis

BiVO4 is an important n-type semiconductor used in photocatalysis due to its high capacity to absorb solar light in the 400–700 nm range, abundance, high chemical stability, non-toxicity, andlow cost. However, research on physicochemical modifications to increase its catalytic activity via simple pr...

Descripción completa

Detalles Bibliográficos
Autores: Aguirre Cortés, Jhon Mauricio, Moral Rodríguez, Adriana Isabel, Bailón García, Esther, Carrasco Marín, Francisco, Pérez Cadenas, Agustín Francisco
Tipo de recurso: artículo
Fecha de publicación:2024
País:España
Institución:Universidad de Castilla-La Mancha
Repositorio:RUIdeRA. Repositorio Institucional de la UCLM
OAI Identifier:oai:ruidera.uclm.es:10578/46906
Acceso en línea:https://doi.org/10.3390/catal14080474
https://www.mdpi.com/2073-4344/14/8/474
https://hdl.handle.net/10578/46906
Access Level:acceso abierto
Palabra clave:BiVO4
Photocatalysts
SMX
Solar light
Descripción
Sumario:BiVO4 is an important n-type semiconductor used in photocatalysis due to its high capacity to absorb solar light in the 400–700 nm range, abundance, high chemical stability, non-toxicity, andlow cost. However, research on physicochemical modifications to increase its catalytic activity via simple procedures is limited. In this work, the influence of different synthesis parameters, such ascalcination temperatures or silver doping, on the structural and physicochemical characteristic of the BiVO4 -based photocatalysts and their photocatalytic performance in degrading sulfamethoxazole from aqueous solution under blue-LED irradiation was evaluated. BiVO4 -based photocatalysts were synthesized using a solvothermal method. The monoclinic phase (m-s) was successfully kept stable even after the thermal treatments at 300, 450, and 600 ?C and the corresponding silver doping. The low bandgap of 2.40 eV and the average particle size of 18 nm of the BiVO4 catalyst treated at 300 ?C seems to be the key. Afte doping, Ag/BiVO4 photocatalyst treated at the optimal found calcination temperature (300 ºC) showed the best photocatalytic behavior.