Amorphous Al-Ti Powders Prepared by Mechanical Alloying and Consolidated by Electrical Resistance Sintering

A novel processing method for amorphous Al50Ti50 alloy, obtained by mechanical alloying and subsequently consolidated by electrical resistance sintering, has been investigated. The characterisation of the powders and the confirmation of the presence of amorphous phase have been carried out by laser...

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Bibliographic Details
Authors: Urban, Petr, Ternero Fernández, Fátima, Caballero, Eduardo S., Nandyala, Sooraj, Montes Martos, Juan Manuel, Gómez Cuevas, Francisco de Paula
Format: article
Publication Date:2019
Country:España
Institution:Universidad de Huelva (UHU)
Repository:Arias Montano. Repositorio Institucional de la Universidad de Huelva
Language:English
OAI Identifier:oai:ariasmontano.uhu.es:10272/17592
Online Access:http://hdl.handle.net/10272/17592
Access Level:Open access
Keyword:Electrical resistance sintering
Amorphisation
Crystallisation
Mechanical alloying
Al-Ti powders
Porosity
Hardness
Description
Summary:A novel processing method for amorphous Al50Ti50 alloy, obtained by mechanical alloying and subsequently consolidated by electrical resistance sintering, has been investigated. The characterisation of the powders and the confirmation of the presence of amorphous phase have been carried out by laser di raction, scanning electron microscopy, X-ray di raction, di erential scanning calorimetry and transmission electron microscopy. The amorphous Al50Ti50 powders, milled for 75 h, have a high hardness and small plastic deformation capacity, not being possible to achieve green compacts for conventional sintering. Moreover, conventional sintering takes a long time, being not possible to avoid crystallisation. Amorphous powders have been consolidated by electrical resistance sintering. Electrically sintered compacts with di erent current intensities (7–8 kA) and processing times (0.8–1.6 s) show a porosity between 16.5 and 20%. The highest Vickers hardness of 662 HV is reached in the centre of an electrically sintered compact with 8 kA and 1.2 s fromamorphous Al50Ti50 powder. The hardness results are compared with the values found in the literature.