The Thermoelectric Properties of Spongy PEDOT Films and 3D-Nanonetworks by Electropolymerization

Recently, polymers have been attracted great attention because of their thermoelectric materials’ excellent mechanical properties, specifically their cost-effectiveness and scalability at the industrial level. In this study, the electropolymerization conditions (applied potential and deposition time...

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Detalles Bibliográficos
Autores: Manzano, Cristina V., Caballero-Calero, Olga, Serrano Rubio, Aída, Resende, Pedro M., Martín-González, Marisol
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2022
País:España
Institución:Consejo Superior de Investigaciones Científicas (CSIC)
Repositorio:DIGITAL.CSIC. Repositorio Institucional del CSIC
OAI Identifier:oai:digital.csic.es:10261/286119
Acceso en línea:http://hdl.handle.net/10261/286119
Access Level:acceso abierto
Palabra clave:PEDOT
Films
3D nanonetworks
Electropolymerization
Thermoelectric properties
Descripción
Sumario:Recently, polymers have been attracted great attention because of their thermoelectric materials’ excellent mechanical properties, specifically their cost-effectiveness and scalability at the industrial level. In this study, the electropolymerization conditions (applied potential and deposition time) of PEDOT films were investigated to improve their thermoelectric properties. The morphology and Raman spectroscopy of the PEDOT films were analyzed according to their applied potential and deposition time. The best thermoelectric properties were found in films grown at 1.3 V for 10 min, with an electrical conductivity of 158 ± 8 S/cm, a Seebeck coefficient of 33 ± 1 µV/K, and a power factor of 17 ± 2 µW/K·m2. This power factor value is three times higher than the value reported in the literature for electropolymerized PEDOT films in acetonitrile using lithium perchlorate as a counter-ion. The thermal conductivity was found to be (1.3 ± 0.3) × 10−1 W/m·K. The highest figure of merit obtained at room temperature was (3.9 ± 1.0) × 10−2 using lithium perchlorate as a counter-ion. In addition, three-dimensional (3D) PEDOT nanonetworks were electropolymerized inside 3D anodic aluminum oxide (3D AAO), obtaining lower values in their thermoelectric properties.