Reduced graphene oxide decorated with SnO2 nanoparticles as negative electrode for lithium ion capacitors

The effort to increase the energy density of conventional electric double-layer capacitors (EDLCs) goes through the development of lithium-ion capacitors (LICs). Herein, we report a self-standing, binder-free composite as the battery-type negative electrode obtained by a low-cost and easily scalable...

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Detalles Bibliográficos
Autores: Arnaiz González, María, Botas, Cristina, Carriazo, Daniel, Mysyk, Roman, Mijangos Antón, Federico, Rojo Aparicio, Teófilo, Ajuria Arregui, Jon, Goikolea Núñez, Eider
Tipo de recurso: artículo
Fecha de publicación:2018
País:España
Institución:Universidad del País Vasco
Repositorio:Addi. Archivo Digital para la Docencia y la Investigación
OAI Identifier:oai:addi.ehu.eus:10810/64834
Acceso en línea:http://hdl.handle.net/10810/64834
Access Level:acceso abierto
Palabra clave:Tin(IV) oxide
reduced graphene oxide
activated carbon
supercapacitor
Lithium-ion capacitor
Descripción
Sumario:The effort to increase the energy density of conventional electric double-layer capacitors (EDLCs) goes through the development of lithium-ion capacitors (LICs). Herein, we report a self-standing, binder-free composite as the battery-type negative electrode obtained by a low-cost and easily scalable method. Tin(IV) oxide nanoparticles (<10 nm) embedded in a reduced graphene oxide matrix (SnO2-rGO) were prepared by an in-situ synthetic approach that involves the freeze/freeze-drying of a graphene oxide suspension in the presence of a tin precursor and its subsequent thermal reduction under argon atmosphere. Physicochemical and electrochemical characterization confirmed the optimum nano-structuration of the composite showing ultrafast response at high current densities. Its coupling with a highly porous olive pits waste-derived activated carbon (AC) as the capacitor-type positive electrode, enables the fabrication of a LIC with an excellent energy density output. The newly designed LIC is able to deliver 60 Wh kg−1 at 2.9 kW kg−1 (tdischarge ≈ 1 min) and still 27 Wh kg−1 at 10.6 kW kg−1 (tdischarge ≈ 10 s).