Immobilized pybox systems as recoverable chiral catalysts

[EN] A simple, versatile and efficient methodology for the immobilization of chiral pybox systems has been developed by formation of a covalent bond between the pyridine ring and the insoluble support using copolymerization (polystyrene-pybox) or grafting (silica gel-pybox). The results indicated th...

Descripción completa

Detalles Bibliográficos
Autores: Cornejo, Alfonso, Fraile, José M., García, José I., Gil, María José, Luis, Santiago V., Martínez-Merino, Víctor, Mayoral, José A.
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2004
País:España
Institución:Consejo Superior de Investigaciones Científicas (CSIC)
Repositorio:DIGITAL.CSIC. Repositorio Institucional del CSIC
OAI Identifier:oai:digital.csic.es:10261/271841
Acceso en línea:http://hdl.handle.net/10261/271841
Access Level:acceso abierto
Palabra clave:Heterogeneous catalysis
Pybox
Catalyse hétérogène
Immobilisation
Copolymerization
Grafting silica gel
Descripción
Sumario:[EN] A simple, versatile and efficient methodology for the immobilization of chiral pybox systems has been developed by formation of a covalent bond between the pyridine ring and the insoluble support using copolymerization (polystyrene-pybox) or grafting (silica gel-pybox). The results indicated that the polymerised pybox offers a behaviour close to that of a homogeneous catalyst. This new route opens the way for the preparation of a range of different supported pybox-based catalysts for a wide variety of enantioselective reactions.