Raman spectroscopy, assisted by X-ray fluorescence and laser-induced breakdown spectroscopy, to characterise original and altered mineral phases in the NWA 2975 Martian shergottite

A fragment of the NWA 2975 Martian meteorite, an enriched basaltic shergottite, was analysed to complete its geochemical characterisation performed 10 years ago. By this means, the feasibility of the employed techniques in a combined way for present and future space exploration missions can be teste...

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Autores: Población, Iratxe, Torre Fernández, Imanol, Aramendia, Julene, López Reyes, Guillermo, Cabalín, Luisa M., Madariaga, Juan Manuel, Rull, Fernando, Laserna, Javier J., Carrizo, Daniel, Martínez Frías , Jesús, Belenguer, Tomás, Belenguer Dávila, Tomás, Taravillo Corralo, Mercedes, Dell'Agliom, Maecella, De Giacomo, Alessandro, Huidobro, Jennifer, Manrique, Jose Antonio, Delgado, Tomás, Arana, Gorka, Castro, Kepa, Veneranda, Marco, Sanz Arranz, J.A., Fortes, F.Javier, García Gómez, Laura
Tipo de recurso: artículo
Fecha de publicación:2023
País:España
Institución:Universidad Complutense de Madrid (UCM)
Repositorio:Docta Complutense
Idioma:inglés
OAI Identifier:oai:docta.ucm.es:20.500.14352/92373
Acceso en línea:https://hdl.handle.net/20.500.14352/92373
Access Level:acceso abierto
Palabra clave:543.426
543.422.2
543.42
523.68
LIBS
micro-Raman spectroscopy
NWA 2975 Martian shergottite
weathering
μ-EDXRF
Óptica (Física)
Física de materiales
2209.19 Óptica Física
2209.21 Espectroscopia
2104.02 Meteoritos
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spelling Raman spectroscopy, assisted by X-ray fluorescence and laser-induced breakdown spectroscopy, to characterise original and altered mineral phases in the NWA 2975 Martian shergottitePoblación, IratxeTorre Fernández, ImanolAramendia, JuleneLópez Reyes, GuillermoCabalín, Luisa M.Madariaga, Juan ManuelRull, FernandoLaserna, Javier J.Carrizo, DanielMartínez Frías , JesúsBelenguer, TomásBelenguer Dávila, TomásTaravillo Corralo, MercedesDell'Agliom, MaecellaDe Giacomo, AlessandroHuidobro, JenniferManrique, Jose AntonioDelgado, TomásArana, GorkaCastro, KepaVeneranda, MarcoSanz Arranz, J.A.Fortes, F.JavierGarcía Gómez, Laura543.426543.422.2543.42523.68LIBSmicro-Raman spectroscopyNWA 2975 Martian shergottiteweatheringμ-EDXRFÓptica (Física)Física de materiales2209.19 Óptica Física2209.21 Espectroscopia2104.02 MeteoritosA fragment of the NWA 2975 Martian meteorite, an enriched basaltic shergottite, was analysed to complete its geochemical characterisation performed 10 years ago. By this means, the feasibility of the employed techniques in a combined way for present and future space exploration missions can be tested. For this aim, Raman spectroscopy was used supported by micro energy dispersive X-ray fluorescence (μ-EDXRF) and laser-induced breakdown spectroscopy (LIBS) for an accurate interpretation of molecular and elemental results. Raman spectroscopy results from two setups, InVia from Renishaw and RLS Simulator, were compared. The major minerals detected by Raman spectroscopy were pyroxenes (mainly augite, pigeonite and enstatite) and plagioclases (mainly shocked maskelynite). Raman spectroscopy allowed defining different metal compositions for these main minerals based on the secondary Raman spectroscopy bands in the 200–500 cm−1 region. In addition, other minerals were found such as merrillite, as well as pyrrhotite and apatite, in several veins and cracks of the meteorite, in agreement with the initial report by the Meteoritical Bulletin. Moreover, it should be highlighted that coesite was found for the very first time in this meteorite.WileyUniversidad Complutense de Madrid20232023-01-0120232023-01-01journal articlehttp://purl.org/coar/resource_type/c_6501VoRhttp://purl.org/coar/version/c_970fb48d4fbd8a85info:eu-repo/semantics/articleapplication/pdfhttps://hdl.handle.net/20.500.14352/92373reponame:Docta Complutenseinstname:Universidad Complutense de Madrid (UCM)Inglésengopen accesshttp://purl.org/coar/access_right/c_abf2Attribution-NonCommercial-NoDerivatives 4.0 Internationalhttp://creativecommons.org/licenses/by-nc-nd/4.0/info:eu-repo/semantics/openAccessoai:docta.ucm.es:20.500.14352/923732026-06-02T12:44:21Z
dc.title.none.fl_str_mv Raman spectroscopy, assisted by X-ray fluorescence and laser-induced breakdown spectroscopy, to characterise original and altered mineral phases in the NWA 2975 Martian shergottite
title Raman spectroscopy, assisted by X-ray fluorescence and laser-induced breakdown spectroscopy, to characterise original and altered mineral phases in the NWA 2975 Martian shergottite
spellingShingle Raman spectroscopy, assisted by X-ray fluorescence and laser-induced breakdown spectroscopy, to characterise original and altered mineral phases in the NWA 2975 Martian shergottite
Población, Iratxe
543.426
543.422.2
543.42
523.68
LIBS
micro-Raman spectroscopy
NWA 2975 Martian shergottite
weathering
μ-EDXRF
Óptica (Física)
Física de materiales
2209.19 Óptica Física
2209.21 Espectroscopia
2104.02 Meteoritos
title_short Raman spectroscopy, assisted by X-ray fluorescence and laser-induced breakdown spectroscopy, to characterise original and altered mineral phases in the NWA 2975 Martian shergottite
title_full Raman spectroscopy, assisted by X-ray fluorescence and laser-induced breakdown spectroscopy, to characterise original and altered mineral phases in the NWA 2975 Martian shergottite
title_fullStr Raman spectroscopy, assisted by X-ray fluorescence and laser-induced breakdown spectroscopy, to characterise original and altered mineral phases in the NWA 2975 Martian shergottite
title_full_unstemmed Raman spectroscopy, assisted by X-ray fluorescence and laser-induced breakdown spectroscopy, to characterise original and altered mineral phases in the NWA 2975 Martian shergottite
title_sort Raman spectroscopy, assisted by X-ray fluorescence and laser-induced breakdown spectroscopy, to characterise original and altered mineral phases in the NWA 2975 Martian shergottite
dc.creator.none.fl_str_mv Población, Iratxe
Torre Fernández, Imanol
Aramendia, Julene
López Reyes, Guillermo
Cabalín, Luisa M.
Madariaga, Juan Manuel
Rull, Fernando
Laserna, Javier J.
Carrizo, Daniel
Martínez Frías , Jesús
Belenguer, Tomás
Belenguer Dávila, Tomás
Taravillo Corralo, Mercedes
Dell'Agliom, Maecella
De Giacomo, Alessandro
Huidobro, Jennifer
Manrique, Jose Antonio
Delgado, Tomás
Arana, Gorka
Castro, Kepa
Veneranda, Marco
Sanz Arranz, J.A.
Fortes, F.Javier
García Gómez, Laura
author Población, Iratxe
author_facet Población, Iratxe
Torre Fernández, Imanol
Aramendia, Julene
López Reyes, Guillermo
Cabalín, Luisa M.
Madariaga, Juan Manuel
Rull, Fernando
Laserna, Javier J.
Carrizo, Daniel
Martínez Frías , Jesús
Belenguer, Tomás
Belenguer Dávila, Tomás
Taravillo Corralo, Mercedes
Dell'Agliom, Maecella
De Giacomo, Alessandro
Huidobro, Jennifer
Manrique, Jose Antonio
Delgado, Tomás
Arana, Gorka
Castro, Kepa
Veneranda, Marco
Sanz Arranz, J.A.
Fortes, F.Javier
García Gómez, Laura
author_role author
author2 Torre Fernández, Imanol
Aramendia, Julene
López Reyes, Guillermo
Cabalín, Luisa M.
Madariaga, Juan Manuel
Rull, Fernando
Laserna, Javier J.
Carrizo, Daniel
Martínez Frías , Jesús
Belenguer, Tomás
Belenguer Dávila, Tomás
Taravillo Corralo, Mercedes
Dell'Agliom, Maecella
De Giacomo, Alessandro
Huidobro, Jennifer
Manrique, Jose Antonio
Delgado, Tomás
Arana, Gorka
Castro, Kepa
Veneranda, Marco
Sanz Arranz, J.A.
Fortes, F.Javier
García Gómez, Laura
author2_role author
author
author
author
author
author
author
author
author
author
author
author
author
author
author
author
author
author
author
author
author
author
author
dc.contributor.none.fl_str_mv Universidad Complutense de Madrid
dc.subject.none.fl_str_mv 543.426
543.422.2
543.42
523.68
LIBS
micro-Raman spectroscopy
NWA 2975 Martian shergottite
weathering
μ-EDXRF
Óptica (Física)
Física de materiales
2209.19 Óptica Física
2209.21 Espectroscopia
2104.02 Meteoritos
topic 543.426
543.422.2
543.42
523.68
LIBS
micro-Raman spectroscopy
NWA 2975 Martian shergottite
weathering
μ-EDXRF
Óptica (Física)
Física de materiales
2209.19 Óptica Física
2209.21 Espectroscopia
2104.02 Meteoritos
description A fragment of the NWA 2975 Martian meteorite, an enriched basaltic shergottite, was analysed to complete its geochemical characterisation performed 10 years ago. By this means, the feasibility of the employed techniques in a combined way for present and future space exploration missions can be tested. For this aim, Raman spectroscopy was used supported by micro energy dispersive X-ray fluorescence (μ-EDXRF) and laser-induced breakdown spectroscopy (LIBS) for an accurate interpretation of molecular and elemental results. Raman spectroscopy results from two setups, InVia from Renishaw and RLS Simulator, were compared. The major minerals detected by Raman spectroscopy were pyroxenes (mainly augite, pigeonite and enstatite) and plagioclases (mainly shocked maskelynite). Raman spectroscopy allowed defining different metal compositions for these main minerals based on the secondary Raman spectroscopy bands in the 200–500 cm−1 region. In addition, other minerals were found such as merrillite, as well as pyrrhotite and apatite, in several veins and cracks of the meteorite, in agreement with the initial report by the Meteoritical Bulletin. Moreover, it should be highlighted that coesite was found for the very first time in this meteorite.
publishDate 2023
dc.date.none.fl_str_mv 2023
2023-01-01
2023
2023-01-01
dc.type.none.fl_str_mv journal article
http://purl.org/coar/resource_type/c_6501
VoR
http://purl.org/coar/version/c_970fb48d4fbd8a85
dc.type.openaire.fl_str_mv info:eu-repo/semantics/article
format article
dc.identifier.none.fl_str_mv https://hdl.handle.net/20.500.14352/92373
url https://hdl.handle.net/20.500.14352/92373
dc.language.none.fl_str_mv Inglés
eng
language_invalid_str_mv Inglés
language eng
dc.rights.none.fl_str_mv open access
http://purl.org/coar/access_right/c_abf2
Attribution-NonCommercial-NoDerivatives 4.0 International
http://creativecommons.org/licenses/by-nc-nd/4.0/
dc.rights.openaire.fl_str_mv info:eu-repo/semantics/openAccess
rights_invalid_str_mv open access
http://purl.org/coar/access_right/c_abf2
Attribution-NonCommercial-NoDerivatives 4.0 International
http://creativecommons.org/licenses/by-nc-nd/4.0/
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
dc.publisher.none.fl_str_mv Wiley
publisher.none.fl_str_mv Wiley
dc.source.none.fl_str_mv reponame:Docta Complutense
instname:Universidad Complutense de Madrid (UCM)
instname_str Universidad Complutense de Madrid (UCM)
reponame_str Docta Complutense
collection Docta Complutense
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