Characterisation of cement pastes with innovative self-healing system based in epoxy-amine adhesive

Two innovative additions are considered for the development of self-healing concrete: epoxy-containing silica microcapsules and amine-functionalized nanosilica. The effect of two concentrations of the additions on the microstructure of a cement paste with silica fume is studied. The results indicate...

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Detalles Bibliográficos
Autores: Pérez Álvarez-Quiñones, Gloria, Gaitero, Juan J., Erkizia, Edurne, Jiménez, Ivelisse, Guerrero Bustos, Ana María
Tipo de recurso: artículo
Estado:Versión aceptada para publicación
Fecha de publicación:2015
País:España
Institución:Consejo Superior de Investigaciones Científicas (CSIC)
Repositorio:DIGITAL.CSIC. Repositorio Institucional del CSIC
OAI Identifier:oai:digital.csic.es:10261/414626
Acceso en línea:http://hdl.handle.net/10261/414626
https://api.elsevier.com/content/abstract/scopus_id/84927938897
Access Level:acceso abierto
Palabra clave:Cementitious material
Characterisation
Nanosilica
Microcapsule
Microstructure
Self-healing
Descripción
Sumario:Two innovative additions are considered for the development of self-healing concrete: epoxy-containing silica microcapsules and amine-functionalized nanosilica. The effect of two concentrations of the additions on the microstructure of a cement paste with silica fume is studied. The results indicate a proper dispersion of the additions within the matrix, a pozzolanic reaction induced by nanosilica and the stability of the microcapsules that reliably isolate the epoxy from the paste. As the concentration of additions increases, a preferential orientation of the portlandite phase is observed, together with a decrease of the compressive strength due to the presence of a minor content of macropores and to the low strength of the capsules. The self-healing efficiency is confirmed in concrete specimens for 150 μm wide cracks and a particular concentration of the additions. These results will be essential for the subsequent development of a reliable self-healing concrete based in the epoxy-amine adhesive.