Design and Optimisation of Sustainable Sample Treatments Based on Ultrasound-Assisted Extraction and Strong Cation-Exchange Purification with Functionalised SBA-15 for Opium Alkaloids in Ground Poppy Seeds

This database includes the results of the optimisation of the analytical methodology, firstly the design of experiments carried out to optimise the extraction step, specifically with ultrasound-assisted extraction, and then the purification step by solid phase extraction. Then all the results obtain...

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Detalles Bibliográficos
Autores: Casado Hidalgo, Gema, Morante Zarcero, Sonia, Pérez Quintanilla, Damián, Sierra Alonso, Isabel
Tipo de recurso: conjunto de datos
Estado:Versión publicada
Fecha de publicación:2023
País:España
Institución:Consorcio Madroño
Repositorio:e-cienciaDatos, Repositorio de Datos del Consorcio Madroño
OAI Identifier:doi:10.21950/FF2SD0
Acceso en línea:https://doi.org/10.21950/FF2SD0
Access Level:acceso abierto
Palabra clave:Chemistry
analytical chemistry
food safety
Opium alkaloids
Ground poppy seeds
Ultrasound-assisted extraction
Solid-phase extraction
SBA-15 functionalised with sulfonic groups
HPLC-MS/MS
Food safety
Natural toxins
Descripción
Sumario:This database includes the results of the optimisation of the analytical methodology, firstly the design of experiments carried out to optimise the extraction step, specifically with ultrasound-assisted extraction, and then the purification step by solid phase extraction. Then all the results obtained from the validation of the analytical methodology and finally the concentrations of opium alkaloids found in samples of ground poppy seeds using the proposed analytical methodology are shown.