V2O5/TiO2 Catalyst for Catalytic Glucose Oxidation to Formic Acid in Batch Reactor: Vanadium Species Nature and Reaction Conditions Optimization

This study focused on the development of vanadium-based catalysts for formic acid production from glucose. The influence of different vanadium precursors on the catalytic activity of titania supported catalysts was contemplated and compared to the performance of commercial and synthesized unsupporte...

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Detalles Bibliográficos
Autores: Álvarez Hernández, Débora, Ivanova, Svetlana, Domínguez Leal, María Isabel, Martínez Blanes, José María, Centeno Gallego, Miguel Ángel
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2024
País:España
Institución:Universidad de Sevilla (US)
Repositorio:idUS. Depósito de Investigación de la Universidad de Sevilla
OAI Identifier:oai:idus.us.es:11441/174039
Acceso en línea:https://hdl.handle.net/11441/174039
https://doi.org/10.1007/s11244-024-01982-0
Access Level:acceso abierto
Palabra clave:Formic acid
Vanadium catalyst
Biomass conversión
Glucose oxidation
Descripción
Sumario:This study focused on the development of vanadium-based catalysts for formic acid production from glucose. The influence of different vanadium precursors on the catalytic activity of titania supported catalysts was contemplated and compared to the performance of commercial and synthesized unsupported V2O5. The obtained results reveal a successful deposition of multiple vanadium species on TiO2 as confirmed by XRD, Raman, and UV-Vis measurements. Catalyst screening identifies V5+ species as main player indicating its important oxidizing potential. Afterwards, the key reaction conditions, as temperature, time, pressure and catalyst loading, were optimized as well as the state of the catalyst after the reaction characterized.