Electronic structure, magnetic properties, and microstructural analysis of thiol-functionalized Au nanoparticles: role of chemical and structural parameters in the ferromagnetic behaviour

Gold nanoparticles (NPs) have been stabilized with a variety of thiol-containing molecules in order to change their chemical and physical properties; among the possible capping systems, alkane chains with different lengths, a carboxylic acid and a thiol-containing biomolecule (tiopronin) have been s...

ver descrição completa

Detalhes bibliográficos
Autores: Guerrero, Estefania, Muñoz Márquez, Miguel, Fernández Pinel, Enrique, Crespo del Arco, Patricia, Hernando Grande, Antonio, Fernández, Asunción
Formato: artículo
Fecha de publicación:2008
País:España
Recursos:Universidad Complutense de Madrid (UCM)
Repositorio:Docta Complutense
Idioma:inglés
OAI Identifier:oai:docta.ucm.es:20.500.14352/52004
Acesso em linha:https://hdl.handle.net/20.500.14352/52004
Access Level:acceso abierto
Palavra-chave:538.9
Capped gold nanoparticles
X-Ray
Tight-binding
Clusters
Spectroscopy
Monolayers
Particles
States
Size
Pd
Física de materiales
Física del estado sólido
2211 Física del Estado Sólido
Descrição
Resumo:Gold nanoparticles (NPs) have been stabilized with a variety of thiol-containing molecules in order to change their chemical and physical properties; among the possible capping systems, alkane chains with different lengths, a carboxylic acid and a thiol-containing biomolecule (tiopronin) have been selected as protecting shells for the synthesized NPs; the NPs solubility in water or organic solvents is determined by the protecting molecule. A full microstructural characterization of these NPs is presented in the current research work. It has been shown that NPs capped with alkanethiol chains have a marked ferromagnetic behaviour which might also be dependent on the chain length. The simultaneous presence of Au-Au and Au-S bonds together with a reduced particle diameter, and the formation of an ordered monolayer protective shell, have proved to be key parameters for the ferromagnetic-like behaviour exhibited by thiol-functionalized gold NPs.