Photoelectrocatalytic detection of NADH on n-type silicon semiconductors facilitated by carbon nanotube fibers

[EN] NADH is a key biomolecule involved in many biocatalytic processes as cofactor and its quantification can be correlated to specific enzymatic activity. Many effort s have been t aken to obt ain clean electrochemical signals related to NADH presence and lower its redox overpotential to avoid inte...

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Detalles Bibliográficos
Autores: Barrio, Melisa del, Rana, Moumita, Vilatela, Juan José, Lorenzo, Encarnación, López de Lacey, Antonio, Pita, Marcos
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2021
País:España
Institución:Consejo Superior de Investigaciones Científicas (CSIC)
Repositorio:DIGITAL.CSIC. Repositorio Institucional del CSIC
OAI Identifier:oai:digital.csic.es:10261/242865
Acceso en línea:http://hdl.handle.net/10261/242865
Access Level:acceso abierto
Palabra clave:NADH detection
Photoelectrochemistry
Carbon nanotube fibers
Semiconductor
Descripción
Sumario:[EN] NADH is a key biomolecule involved in many biocatalytic processes as cofactor and its quantification can be correlated to specific enzymatic activity. Many effort s have been t aken to obt ain clean electrochemical signals related to NADH presence and lower its redox overpotential to avoid interferences. Suppression of background and secondary signals can be achieved by including a switchable electroactive surface, for instance, by using semiconductors able to harvest light energy and drive the excited electrons only when irradiated. Here we present the combination of a n-type Si semiconductor with fibers made of carbon nanotubes as electroactive surface for NADH quantification at low potentials only upon irradiation. The resulting photoelectrode responded linearly to NADH concentrations from 50 μM to 1.6 mM with high sensitivity (54 μA cm −2 mM −1 ). This system may serve as a biosensing platform for detection and quantification of dehydrogenases’ activity.