Crystal structure of (1,3-di-tert-butyl- η 5-cyclo­penta­dien­yl)tri­methyl­hafnium(IV)

The mol­ecule of the title organometallic hafnium(IV) com­pound, [Hf(CH3) 3(C 13H 21)] or [HfMe3( η 5-C 5H 3-1,3- tBu 2)], adopts the classical three-legged piano-stool geometry for mono­cyclo­penta­dienylhafnium(IV) derivatives with the three methyl groups bonded to the Hf(IV) atom at the legs. The...

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Detalles Bibliográficos
Autores: Pérez Redondo, Adrián, Varela-Izquierdo, Víctor, Yélamos, Carlos
Tipo de recurso: conjunto de datos
Estado:Versión publicada
Fecha de publicación:2019
País:España
Institución:Consorcio Madroño
Repositorio:e-cienciaDatos, Repositorio de Datos del Consorcio Madroño
OAI Identifier:doi:10.21950/BCYB9Y
Acceso en línea:https://doi.org/10.21950/BCYB9Y
Access Level:acceso abierto
Palabra clave:Chemistry
Crystal structure
Hafnium
Cyclo­penta­dienyl ligand
Organometallic compound.
Descripción
Sumario:The mol­ecule of the title organometallic hafnium(IV) com­pound, [Hf(CH3) 3(C 13H 21)] or [HfMe3( η 5-C 5H 3-1,3- tBu 2)], adopts the classical three-legged piano-stool geometry for mono­cyclo­penta­dienylhafnium(IV) derivatives with the three methyl groups bonded to the Hf(IV) atom at the legs. The C atoms of the two tert-butyl group bonded to the cyclo­penta­dienyl (Cp) ring are 0.132 (5) and 0.154 (6) Å above the Cp least-squares plane. There are no significant inter­molecular inter­actions present between the mol­ecules in the crystal structure.